Growth behavior of TiB 2 hexagonal plates prepared via a molten‐salt‐mediated carbothermal reduction

TiB 2 powders were successfully synthesized by a molten‐salt‐mediated carbothermal reduction method. The products obtained at 1300°C for 2 hours were hexagonal plates with side length of 3‐8 μm and thicknesses of 200‐500 nm. The microstructural evolution with temperature confirmed that the growth of...

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Published in:Journal of the American Ceramic Society 2020-02, Vol.103 (2), p.719-723
Main Authors: Song, Shaolei, Zhang, Tong, Xie, Chen, Zhou, Jianmin, Li, Rong, Zhen, Qiang
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Language:English
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description TiB 2 powders were successfully synthesized by a molten‐salt‐mediated carbothermal reduction method. The products obtained at 1300°C for 2 hours were hexagonal plates with side length of 3‐8 μm and thicknesses of 200‐500 nm. The microstructural evolution with temperature confirmed that the growth of TiB 2 hexagonal plates was a layer‐by‐layer growth controlled by a two‐dimensional nucleation. No‐uniform grains were observed attached on side and step edges of TiB 2 plates, which became finer and disappeared during the growth. This indicated that layer growth and growth on the side of TiB 2 plates followed the surface adsorption growth model.
doi_str_mv 10.1111/jace.16800
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title Growth behavior of TiB 2 hexagonal plates prepared via a molten‐salt‐mediated carbothermal reduction
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