Structure of 1,10-diazonium-18-crown-6 bis(tetrafluoroborate)

The interaction of 1,10-diaza-18-crown-6 (L) with boron trifluoride etherate results in the formation of a complex of the composition (LH 2 )[BF 4 ] 2 whose structure is established by single crystal X-ray diffraction. The supramolecular structure of the perching type complex is stabilized by interi...

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Bibliographic Details
Published in:Journal of structural chemistry 2014-11, Vol.55 (6), p.1125-1127
Main Authors: Gelmboldt, V. O., Ganin, E‘. V., Lipkowski, J., Fonari, M. S.
Format: Article
Language:English
Subjects:
Atomic
Atomic/Molecular Structure and Spectra
Brief Communications
Chemistry
Chemistry and Materials Science
Inorganic Chemistry
Molecular
Optical and Plasma Physics
Physical Chemistry
Solid State Physics
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Summary:The interaction of 1,10-diaza-18-crown-6 (L) with boron trifluoride etherate results in the formation of a complex of the composition (LH 2 )[BF 4 ] 2 whose structure is established by single crystal X-ray diffraction. The supramolecular structure of the perching type complex is stabilized by interionic NH⋯F H-bonds (N⋯F 2.715(11)-2.964(9) Å).
ISSN:0022-4766
1573-8779
DOI:10.1134/S0022476614060201