Crystal structure of N′-pivaloyl-N-phenylpivalohydrazide

A novel hydrazide compound (C 16 H 24 N 2 O 2 ) is synthesized in a single step by the reaction of pivaloyl chloride with phenylhydrazine in a 2:1 molar ratio in dry DCM. The molecular structure is determined by the single crystal X-ray analysis. The compound crystallized in the monoclinic system, s...

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Bibliographic Details
Published in:Journal of structural chemistry 2015-03, Vol.56 (2), p.396-398
Main Authors: Saeed, A., Arshad, I., Flörke, U.
Format: Article
Language:English
Subjects:
Atomic
Atomic/Molecular Structure and Spectra
Chemistry
Chemistry and Materials Science
Inorganic Chemistry
Molecular
Optical and Plasma Physics
Physical Chemistry
Solid State Physics
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Summary:A novel hydrazide compound (C 16 H 24 N 2 O 2 ) is synthesized in a single step by the reaction of pivaloyl chloride with phenylhydrazine in a 2:1 molar ratio in dry DCM. The molecular structure is determined by the single crystal X-ray analysis. The compound crystallized in the monoclinic system, space group P 2 1 / c with a = 15.4638(17) Å, b = 9.9481(11) Å, c = 10.5276(12) Å, β = 90.194(3)°, Z = 4, V = 1619.5(3) Å 3 .
ISSN:0022-4766
1573-8779
DOI:10.1134/S0022476615020304