Synthesis and characterization of new ammonium-containing niobium fluoro complexes of composition NH₄NaNbF₇ and NH₄MNbOF₅ (M = Li and Na)

Ammonium-containing mixed-alkali-metal fluoro complexes NH₄NaNbF₇ and NH₄MNbOF₅ (M = Li and Na) crystallizing in orthorhombic system were synthesized and characterized for the first time. Unit cell parameters for these complexes were determined. Their IR absorption spectra were measured and characte...

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Bibliographic Details
Published in:Russian journal of inorganic chemistry 2010-05, Vol.55 (5), p.655-660
Main Authors: Antokhina, T. F, Savchenko, N. N, Ignat'eva, L. N, Kaidalova, T. A
Format: Article
Language:English
Subjects:
Chemistry
Chemistry and Materials Science
Inorganic Chemistry
Synthesis and Properties of Inorganic Compounds
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Summary:Ammonium-containing mixed-alkali-metal fluoro complexes NH₄NaNbF₇ and NH₄MNbOF₅ (M = Li and Na) crystallizing in orthorhombic system were synthesized and characterized for the first time. Unit cell parameters for these complexes were determined. Their IR absorption spectra were measured and characterized in the range 4000-350 cm⁻¹.
ISSN:0036-0236
1531-8613
DOI:10.1134/S0036023610050013