The composition of commercial acetylated glycerol samples determined by 13C and 1H NMR. The comparison with gas chromatography

A convenient method for the analysis of commercial acetylated glycerol samples based on 13 C NMR is presented with the accuracy comparable to the standard gas chromatography approaches. The advantage of method is that it does not need any sample derivatization procedure by silyl groups and its appli...

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Bibliographic Details
Published in:Journal of analytical chemistry (New York, N.Y.) N.Y.), 2014-08, Vol.69 (8), p.763-768
Main Authors: Sustere, Z., Kampare, R., Liepins, E., Kampars, V.
Format: Article
Language:English
Subjects:
Analytical Chemistry
Chemistry
Chemistry and Materials Science
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Summary:A convenient method for the analysis of commercial acetylated glycerol samples based on 13 C NMR is presented with the accuracy comparable to the standard gas chromatography approaches. The advantage of method is that it does not need any sample derivatization procedure by silyl groups and its application is much more straightforward, as compared to the published 1 H NMR method.
ISSN:1061-9348
1608-3199
DOI:10.1134/S1061934814080103