Chromatographic determination of C70 fullerene in animal organs and tissues

A method has been developed for the determination of C₇₀ fullerene in animal organs and tissues using reversed-phase high-performance liquid chromatography with ultraviolet detection combined with sample preparation consisting in the homogenization of samples, treatment of the homogenates with aceti...

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Bibliographic Details
Published in:Journal of analytical chemistry (New York, N.Y.) N.Y.), 2015-12, Vol.70 (12), p.1507-1511
Main Authors: Morozova, O. V, Vasil’eva, I. S, Shumakovich, G. P, Sof’in, A. V, Hendrickson, O. D, Zherdev, A. V, Dzantiev, B. B, Yaropolov, A. I
Format: Article
Language:English
Subjects:
acetic acid
Analytical Chemistry
animal organs
Chemistry
Chemistry and Materials Science
detection limit
fullerene
homogenization
reversed-phase high performance liquid chromatography
tissues
toluene
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Summary:A method has been developed for the determination of C₇₀ fullerene in animal organs and tissues using reversed-phase high-performance liquid chromatography with ultraviolet detection combined with sample preparation consisting in the homogenization of samples, treatment of the homogenates with acetic acid, and extraction of fullerene with toluene. The recovery of C₇₀ fullerene from various organs was ~89–93%, the limit of detection is 75 ng/mL.
ISSN:1061-9348
1608-3199
DOI:10.1134/S1061934815120138