Reactions of 1-bromo-1-nitro-3,3,3-trichloropropene with acetylacetone and cyclohexane-1,3-dione

Reactions of 1-bromo-1-nitro-3,3,3-trichloropropene with acetylacetone, dihydroresorcinol, and dimedone afforded substituted dihydrofuran and hexahydrobenzofurans containing nitro and trichloromethyl functionalities. Their structure was established by spectroscopic (IR, UV, 1 H, 13 C–{ 1 H} NMR) met...

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Bibliographic Details
Published in:Russian journal of general chemistry 2015-10, Vol.85 (10), p.2291-2294
Main Authors: Makarenko, S. V., Stukan’, E. V., Trukhin, E. V., Berestovitskaya, V. M.
Format: Article
Language:English
Subjects:
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
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Summary:Reactions of 1-bromo-1-nitro-3,3,3-trichloropropene with acetylacetone, dihydroresorcinol, and dimedone afforded substituted dihydrofuran and hexahydrobenzofurans containing nitro and trichloromethyl functionalities. Their structure was established by spectroscopic (IR, UV, 1 H, 13 C–{ 1 H} NMR) methods and X-ray diffraction analysis.
ISSN:1070-3632
1608-3350
DOI:10.1134/S1070363215100126