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31P{27Al} MQMAS/HETCOR NMR Study on Structure of Amorphous AlPO4
A solid-state NMR method combining 27Al multiple-quantum magic-angle spinning (MQMAS) and 31P{27Al} heteronuclear correlation (HETCOR) has been applied for the structural analysis of amorphous AlPO4. We obtained a correlation between the isotropic chemical shifts of 31P in PO4 and of 27Al in each Al...
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Published in: | Chemistry letters 2005-10, Vol.34 (10), p.1380-1381 |
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Main Authors: | , , , , , , |
Format: | Article |
Language: | English |
Citations: | Items that this one cites Items that cite this one |
Online Access: | Get full text |
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Summary: | A solid-state NMR method combining 27Al multiple-quantum magic-angle spinning (MQMAS) and 31P{27Al} heteronuclear correlation (HETCOR) has been applied for the structural analysis of amorphous AlPO4. We obtained a correlation between the isotropic chemical shifts of 31P in PO4 and of 27Al in each AlOn (n = 4, 5, and 6) distributed by the amorphous structure. |
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ISSN: | 0366-7022 1348-0715 |
DOI: | 10.1246/cl.2005.1380 |