DBU-Promoted Cu(OAc)•H 2 O-Catalysed Coupling Reactions of Aryl Iodides and Sodium Azide

An efficient and simple protocol for the synthesis of aryl azides by the coupling of aryl iodides with sodium azide, in good to excellent yields in DMSO at 95 °C under catalysis by Cu(OAc) 2 -H 2 O and 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU), has been established. The optimised loadings of Cu(OAc)...

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Published in:Journal of chemical research 2018-06, Vol.42 (5), p.247-250
Main Authors: Jiang, Yuqin, Suo, Huajun, Zhao, Yaru, Li, Xiyong, Sun, Yamin, Li, Xingfeng, Dong, Wenpei, Li, Wei, Zhang, Weiwei, Xu, Guiqing
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container_end_page 250
container_issue 5
container_start_page 247
container_title Journal of chemical research
container_volume 42
creator Jiang, Yuqin
Suo, Huajun
Zhao, Yaru
Li, Xiyong
Sun, Yamin
Li, Xingfeng
Dong, Wenpei
Li, Wei
Zhang, Weiwei
Xu, Guiqing
description An efficient and simple protocol for the synthesis of aryl azides by the coupling of aryl iodides with sodium azide, in good to excellent yields in DMSO at 95 °C under catalysis by Cu(OAc) 2 -H 2 O and 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU), has been established. The optimised loadings of Cu(OAc) 2 -H 2 O and DBU were 10 mol% and 15 mol% respectively.
doi_str_mv 10.3184/174751918X15260507766192
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title DBU-Promoted Cu(OAc)•H 2 O-Catalysed Coupling Reactions of Aryl Iodides and Sodium Azide
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