Loading…

rac -Diethyl 9-hydroxy-9-methyl-7-phenyl-1,4-diazaspiro[4.5]decane-6,8-dicarboxylate

The title molecule, C21H30N2O5, is chiral with four stereogenic centres. The crystal is a racemate and consists of enantiomeric pairs with the relative configuration rac-(6S*,7R*,8R*,9S*). The ethyl fragment of the ethoxycarbonyl group at position 6 is disordered in a 0.46 (3):0.54&#81...

Full description

Saved in:
Bibliographic Details
Published in:Acta crystallographica. Section E, Structure reports online Structure reports online, 2011-02, Vol.67 (2), p.o291-o291
Main Authors: Maharramov, Abel M., Ismiyev, Arif I., Rashidov, Bahruz A., Rahimova, Gunel M., Allahverdiyev, Mirza A.
Format: Article
Language:English
Citations: Items that cite this one
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
cited_by cdi_FETCH-LOGICAL-c354t-b0e393d733ddaa0397f6928f3c209b6a5810a9cd61ccd417947ad960b41aa90c3
cites
container_end_page o291
container_issue 2
container_start_page o291
container_title Acta crystallographica. Section E, Structure reports online
container_volume 67
creator Maharramov, Abel M.
Ismiyev, Arif I.
Rashidov, Bahruz A.
Rahimova, Gunel M.
Allahverdiyev, Mirza A.
description The title molecule, C21H30N2O5, is chiral with four stereogenic centres. The crystal is a racemate and consists of enantiomeric pairs with the relative configuration rac-(6S*,7R*,8R*,9S*). The ethyl fragment of the ethoxycarbonyl group at position 6 is disordered in a 0.46 (3):0.54 (3) ratio. The crystal structure features intermolecular N—H...O. Intramolecular O—H...N and N—H...O hydrogen bonds also occur.
doi_str_mv 10.1107/S1600536810054498
format article
fullrecord <record><control><sourceid>doaj_cross</sourceid><recordid>TN_cdi_doaj_primary_oai_doaj_org_article_11dc784427f24963a43a15dc481127f3</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><doaj_id>oai_doaj_org_article_11dc784427f24963a43a15dc481127f3</doaj_id><sourcerecordid>oai_doaj_org_article_11dc784427f24963a43a15dc481127f3</sourcerecordid><originalsourceid>FETCH-LOGICAL-c354t-b0e393d733ddaa0397f6928f3c209b6a5810a9cd61ccd417947ad960b41aa90c3</originalsourceid><addsrcrecordid>eNplkF1LwzAUhoMoOKc_wLv9gGXmNGnSXMr8Ggy8cF6JhNMktR3dWtJeWH-96SYieHVensN54LyEXANbADB18wKSsZTLDOIQQmcnZDIiOrLTP_mcXHTdljGQKoEJ2QS0M3pX-b4c6pmm5eBC8zlQTXcHRBVtS7-PAeaCugq_sGur0LyJRfruvMW9p3KexY3FkMfLGnt_Sc4KrDt_9TOn5PXhfrN8ouvnx9Xydk0tT0VPc-a55k5x7hwi41oVUidZwW3CdC4xjc-gtk6CtU6A0kKh05LlAhA1s3xKVkeva3Br2lDtMAymwcocQBM-DIa-srU3AM6qTIhEFYnQkqPgCKmzIgOIjEcXHF02NF0XfPHrA2bGis2_ivk3j3hrrA</addsrcrecordid><sourcetype>Open Website</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>rac -Diethyl 9-hydroxy-9-methyl-7-phenyl-1,4-diazaspiro[4.5]decane-6,8-dicarboxylate</title><source>PubMed Central(OpenAccess)</source><creator>Maharramov, Abel M. ; Ismiyev, Arif I. ; Rashidov, Bahruz A. ; Rahimova, Gunel M. ; Allahverdiyev, Mirza A.</creator><creatorcontrib>Maharramov, Abel M. ; Ismiyev, Arif I. ; Rashidov, Bahruz A. ; Rahimova, Gunel M. ; Allahverdiyev, Mirza A.</creatorcontrib><description>The title molecule, C21H30N2O5, is chiral with four stereogenic centres. The crystal is a racemate and consists of enantiomeric pairs with the relative configuration rac-(6S*,7R*,8R*,9S*). The ethyl fragment of the ethoxycarbonyl group at position 6 is disordered in a 0.46&amp;#8197;(3):0.54&amp;#8197;(3) ratio. The crystal structure features intermolecular N&amp;#8212;H...O. Intramolecular O&amp;#8212;H...N and N&amp;#8212;H...O hydrogen bonds also occur.</description><identifier>ISSN: 1600-5368</identifier><identifier>EISSN: 1600-5368</identifier><identifier>DOI: 10.1107/S1600536810054498</identifier><language>eng</language><publisher>International Union of Crystallography</publisher><ispartof>Acta crystallographica. Section E, Structure reports online, 2011-02, Vol.67 (2), p.o291-o291</ispartof><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c354t-b0e393d733ddaa0397f6928f3c209b6a5810a9cd61ccd417947ad960b41aa90c3</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Maharramov, Abel M.</creatorcontrib><creatorcontrib>Ismiyev, Arif I.</creatorcontrib><creatorcontrib>Rashidov, Bahruz A.</creatorcontrib><creatorcontrib>Rahimova, Gunel M.</creatorcontrib><creatorcontrib>Allahverdiyev, Mirza A.</creatorcontrib><title>rac -Diethyl 9-hydroxy-9-methyl-7-phenyl-1,4-diazaspiro[4.5]decane-6,8-dicarboxylate</title><title>Acta crystallographica. Section E, Structure reports online</title><description>The title molecule, C21H30N2O5, is chiral with four stereogenic centres. The crystal is a racemate and consists of enantiomeric pairs with the relative configuration rac-(6S*,7R*,8R*,9S*). The ethyl fragment of the ethoxycarbonyl group at position 6 is disordered in a 0.46&amp;#8197;(3):0.54&amp;#8197;(3) ratio. The crystal structure features intermolecular N&amp;#8212;H...O. Intramolecular O&amp;#8212;H...N and N&amp;#8212;H...O hydrogen bonds also occur.</description><issn>1600-5368</issn><issn>1600-5368</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><sourceid>DOA</sourceid><recordid>eNplkF1LwzAUhoMoOKc_wLv9gGXmNGnSXMr8Ggy8cF6JhNMktR3dWtJeWH-96SYieHVensN54LyEXANbADB18wKSsZTLDOIQQmcnZDIiOrLTP_mcXHTdljGQKoEJ2QS0M3pX-b4c6pmm5eBC8zlQTXcHRBVtS7-PAeaCugq_sGur0LyJRfruvMW9p3KexY3FkMfLGnt_Sc4KrDt_9TOn5PXhfrN8ouvnx9Xydk0tT0VPc-a55k5x7hwi41oVUidZwW3CdC4xjc-gtk6CtU6A0kKh05LlAhA1s3xKVkeva3Br2lDtMAymwcocQBM-DIa-srU3AM6qTIhEFYnQkqPgCKmzIgOIjEcXHF02NF0XfPHrA2bGis2_ivk3j3hrrA</recordid><startdate>20110201</startdate><enddate>20110201</enddate><creator>Maharramov, Abel M.</creator><creator>Ismiyev, Arif I.</creator><creator>Rashidov, Bahruz A.</creator><creator>Rahimova, Gunel M.</creator><creator>Allahverdiyev, Mirza A.</creator><general>International Union of Crystallography</general><scope>AAYXX</scope><scope>CITATION</scope><scope>DOA</scope></search><sort><creationdate>20110201</creationdate><title>rac -Diethyl 9-hydroxy-9-methyl-7-phenyl-1,4-diazaspiro[4.5]decane-6,8-dicarboxylate</title><author>Maharramov, Abel M. ; Ismiyev, Arif I. ; Rashidov, Bahruz A. ; Rahimova, Gunel M. ; Allahverdiyev, Mirza A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c354t-b0e393d733ddaa0397f6928f3c209b6a5810a9cd61ccd417947ad960b41aa90c3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><toplevel>online_resources</toplevel><creatorcontrib>Maharramov, Abel M.</creatorcontrib><creatorcontrib>Ismiyev, Arif I.</creatorcontrib><creatorcontrib>Rashidov, Bahruz A.</creatorcontrib><creatorcontrib>Rahimova, Gunel M.</creatorcontrib><creatorcontrib>Allahverdiyev, Mirza A.</creatorcontrib><collection>CrossRef</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>Acta crystallographica. Section E, Structure reports online</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Maharramov, Abel M.</au><au>Ismiyev, Arif I.</au><au>Rashidov, Bahruz A.</au><au>Rahimova, Gunel M.</au><au>Allahverdiyev, Mirza A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>rac -Diethyl 9-hydroxy-9-methyl-7-phenyl-1,4-diazaspiro[4.5]decane-6,8-dicarboxylate</atitle><jtitle>Acta crystallographica. Section E, Structure reports online</jtitle><date>2011-02-01</date><risdate>2011</risdate><volume>67</volume><issue>2</issue><spage>o291</spage><epage>o291</epage><pages>o291-o291</pages><issn>1600-5368</issn><eissn>1600-5368</eissn><abstract>The title molecule, C21H30N2O5, is chiral with four stereogenic centres. The crystal is a racemate and consists of enantiomeric pairs with the relative configuration rac-(6S*,7R*,8R*,9S*). The ethyl fragment of the ethoxycarbonyl group at position 6 is disordered in a 0.46&amp;#8197;(3):0.54&amp;#8197;(3) ratio. The crystal structure features intermolecular N&amp;#8212;H...O. Intramolecular O&amp;#8212;H...N and N&amp;#8212;H...O hydrogen bonds also occur.</abstract><pub>International Union of Crystallography</pub><doi>10.1107/S1600536810054498</doi><oa>free_for_read</oa></addata></record>
fulltext fulltext
identifier ISSN: 1600-5368
ispartof Acta crystallographica. Section E, Structure reports online, 2011-02, Vol.67 (2), p.o291-o291
issn 1600-5368
1600-5368
language eng
recordid cdi_doaj_primary_oai_doaj_org_article_11dc784427f24963a43a15dc481127f3
source PubMed Central(OpenAccess)
title rac -Diethyl 9-hydroxy-9-methyl-7-phenyl-1,4-diazaspiro[4.5]decane-6,8-dicarboxylate
url http://sfxeu10.hosted.exlibrisgroup.com/loughborough?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-29T09%3A36%3A25IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-doaj_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=rac%20-Diethyl%209-hydroxy-9-methyl-7-phenyl-1,4-diazaspiro%5B4.5%5Ddecane-6,8-dicarboxylate&rft.jtitle=Acta%20crystallographica.%20Section%20E,%20Structure%20reports%20online&rft.au=Maharramov,%20Abel%20M.&rft.date=2011-02-01&rft.volume=67&rft.issue=2&rft.spage=o291&rft.epage=o291&rft.pages=o291-o291&rft.issn=1600-5368&rft.eissn=1600-5368&rft_id=info:doi/10.1107/S1600536810054498&rft_dat=%3Cdoaj_cross%3Eoai_doaj_org_article_11dc784427f24963a43a15dc481127f3%3C/doaj_cross%3E%3Cgrp_id%3Ecdi_FETCH-LOGICAL-c354t-b0e393d733ddaa0397f6928f3c209b6a5810a9cd61ccd417947ad960b41aa90c3%3C/grp_id%3E%3Coa%3E%3C/oa%3E%3Curl%3E%3C/url%3E&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true