Complete Desorption of Hybrid Nanoclays Composed of Hydrotalcite and Disperse Dye

Clays are considered great nanoadsorbents for many materials, including textile dyes. The use of these materials for cleaning textile wastewater is well known; however, it is not at all common to find applications for the hybrid materials formed from the clay and dye. In this work, a dye-loaded clay...

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Bibliographic Details
Published in:International journal of molecular sciences 2023-06, Vol.24 (13), p.10950
Main Authors: López-Rodríguez, Daniel, Micó-Vicent, Bàrbara, Jordán-Núñez, Jorge, Montava-Seguí, Ignacio, Bou-Belda, Eva
Format: Article
Language:English
Subjects:
Adsorption
Analysis
Clay
Color fastness
Coloring Agents - chemistry
Desorption
disperse dye recovery
Dispersion
dye adsorption
Dyeing
Dyes
fastness colour dyeing clay
hydrotalcite
Infrared analysis
Infrared spectroscopy
nanoclay dyeing
Photoelectron spectroscopy
Photoelectrons
Polyesters
Porosity
Reagents
removal of dyes
Stability analysis
Textiles
Thermogravimetry
Wastewater
X ray photoelectron spectroscopy
X-ray diffraction
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Summary:Clays are considered great nanoadsorbents for many materials, including textile dyes. The use of these materials for cleaning textile wastewater is well known; however, it is not at all common to find applications for the hybrid materials formed from the clay and dye. In this work, a dye-loaded clay material was used to make new dye baths and colour a polyester textile substrate. The same hybrid could be used several times as it did not use all the adsorbed dye in a single dyeing. The hybrid obtained from hydrotalcite (nanoclay) and the dispersed red 1 dye was analysed by measuring the colour obtained, carrying out an X-ray diffraction analysis that provided information after each desorption-dyeing process, and using infrared spectroscopy to analyse the specific bands of each characteristic group. Both analyses showed that the amount of dye present in the hybrid decreases. Thermogravimetry (TGA), surface area and porosity measurements (BET), and X-ray photoelectron spectroscopy (XPS) tests were conducted. Chemical stability was assessed by subjecting the hybrid to the actions of different reagents. In addition, colour fastness tests were carried out after dyeing and washing the polyester test tubes to check for the correct fixing of the dye to the fibre. These fastness results showed that the dyeing was carried out correctly and as if it was a conventional dyeing process.
ISSN:1422-0067
1661-6596
1422-0067
DOI:10.3390/ijms241310950