14-(1,3-Benzodioxol-5-yl)-7,14-dihydrodibenzo[ a , j ]acridine

The title compound, C28H19NO2, was synthesized by the reaction of 1,3-benzodioxole-5-carbaldehyde with naphthalen-2-amine catalyzed by thiosalicylic acid in acetic acid. The central dihydropyridine ring adopts a boat conformation. The two planar (r.m.s. deviations = 0.0158 and 0.0552 &...

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Bibliographic Details
Published in:Acta crystallographica. Section E, Structure reports online Structure reports online, 2010-12, Vol.66 (12), p.o3073-o3073
Main Authors: Jia, Runhong, Peng, Juhua, Tu, ShuJiang
Format: Article
Language:English
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Summary:The title compound, C28H19NO2, was synthesized by the reaction of 1,3-benzodioxole-5-carbaldehyde with naphthalen-2-amine catalyzed by thiosalicylic acid in acetic acid. The central dihydropyridine ring adopts a boat conformation. The two planar (r.m.s. deviations = 0.0158 and 0.0552 Å) bicyclic parts make a dihedral angle of 16.16 (5)° with respect to each other. The crystal packing is stabilized by intermolecular N—H...O hydrogen bonds and C—H...π interactions.
ISSN:1600-5368
1600-5368
DOI:10.1107/S1600536810044302