1,3-Bis(2-ethoxy-phen-yl)triazene methanol 0.33-solvate

There are three independent mol-ecules of 1,3-bis-(2-ethoxy-phen-yl)triazene and a mol-ecule of methanol in the asymmetric unit of the title compound, C(16)H(19)N(3)O(2)·0.33CH(3)OH. Two mol-ecules related by a non-crystallographic pseudo-twofold rotation axis are linked via distinct inter-molecular...

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Published in:Acta crystallographica. Section E, Structure reports online Structure reports online, 2009-09, Vol.65 (Pt 10), p.o2391-o2391
Main Authors: Rofouei, Mohammad Kazem, Melardi, Mohammad Reza, Salemi, Yasaman, Attar Gharamaleki, Jafar
Format: Article
Language:English
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Organic Papers
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Summary:There are three independent mol-ecules of 1,3-bis-(2-ethoxy-phen-yl)triazene and a mol-ecule of methanol in the asymmetric unit of the title compound, C(16)H(19)N(3)O(2)·0.33CH(3)OH. Two mol-ecules related by a non-crystallographic pseudo-twofold rotation axis are linked via distinct inter-molecular N-H⋯N hydrogen bonds, leading to the formation of a dimer with an R(2) (2)(8) graph set. The third mol-ecule is connected to the methanol mol-ecule by O-H⋯N and N-H⋯O hydrogen bonds. There are a number of weak C-H⋯π inter-actions, with H⋯π distances ranging from 2.74 to 2.89 Å between the C-H groups and the aromatic benzene rings.
ISSN:1600-5368
1600-5368
DOI:10.1107/S1600536809035338