2,3,5,6-Tetrafluoro-[N-(3-aminopropyl)-ε-caprolactam]-4-pyridine

The title compound was synthesized at a near-quantitative yield using the nucleophilic aromatic substitution of 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) with perfluoropyridine (PFP). The purity and structure were determined by NMR (1H, 13C, 19F), GC-EIMS, and single-crystal X-ray crystallography.

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Bibliographic Details
Published in:MolBank 2024-03, Vol.2024 (1), p.M1777
Main Authors: Friesen, Chadron M., Weeks, Nathan J., Iacono, Scott T.
Format: Article
Language:English
Subjects:
1,8-diazabicyclo[5.4.0]undec-7-ene (DBU)
Caprolactam
Carbon
Crystallography
NMR
Nuclear magnetic resonance
nucleophilic aromatic substitution
organo-fluorine
pentafluoropyridine
pyridine
Single crystals
Software
Solvents
Citations: Items that this one cites
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Description
Summary:The title compound was synthesized at a near-quantitative yield using the nucleophilic aromatic substitution of 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) with perfluoropyridine (PFP). The purity and structure were determined by NMR (1H, 13C, 19F), GC-EIMS, and single-crystal X-ray crystallography.
ISSN:1422-8599
1422-8599
DOI:10.3390/M1777