Improved Synthesis of 1-O-Acyl-β-d-Glucopyranose Tetraacetates

An improved synthesis of 1- -acyl glucosyl esters that avoids the use of expensive Ag reagents as well as the hydrolysis of unstable glucosyl bromides is reported. Notably, β-configuration products were obtained exclusively in good yields.

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Bibliographic Details
Published in:Molecules (Basel, Switzerland) Switzerland), 2017-04, Vol.22 (4), p.662
Main Authors: Chen, Yu, Lu, Huan, Chen, Yanyu, Yu, Wansheng, Dai, Hui, Pan, Xianhua
Format: Article
Language:English
Subjects:
Acetates - chemical synthesis
Acetates - chemistry
aliphatic acids
aromatic acids
Brand names
Cosmetics
Esters - chemical synthesis
Fatty acids
Fluorides
Glucosides - chemical synthesis
Glucosides - chemistry
glucosyl bromide
glucosyl esters
Hydrolysis
Magnetic Resonance Spectroscopy
Medical supplies
Reagents
Structure-Activity Relationship
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Description
Summary:An improved synthesis of 1- -acyl glucosyl esters that avoids the use of expensive Ag reagents as well as the hydrolysis of unstable glucosyl bromides is reported. Notably, β-configuration products were obtained exclusively in good yields.
ISSN:1420-3049
1420-3049
DOI:10.3390/molecules22040662