In situ characterization of high-temperature mechanical behaviors of freestanding Si, BSAS and Yb2SiO5 environmental barrier coatings by three-point bending tests based on digital image correlation

• Published in: Results in surfaces and interfaces 2023-08, Vol.12, p.100130, Article 100130
• Main Authors: Fan, Xizhi, Deng, Xixing, Mao, Weiguo, Luo, Zhangji, Ye, Wenjie, Dai, Cuiying
• Format: Article
• Language: English
• Subjects: Digital image correlation method; Environmental barrier coatings; High-temperature mechanical properties; In situ characterization; Three-point bending
• ISSN: 2666-8459; 2666-8459
• DOI: 10.1016/j.rsurfi.2023.100130

The high-temperature mechanical properties and failure mechanisms of Si, BSAS and Yb2SiO5 ceramic materials are important for environmental barrier coatings. The Si coating, BSAS coating and Yb2SiO5 coating were prepared by the atmospheric plasma spray (APS) technique. The elastic modulus, fracture strength and fracture strain are determined by three-point bending combined with the digital image correlation (DIC) method. The results show that as the test temperature increases from 25 °C to 1000 °C, the elastic modulus of the Si coating and Yb2SiO5 coating decreases while the elastic modulus of the BSAS coating increases. And the fracture strength and fracture strain of the Si coating, BSAS coating and Yb2SiO5 coating increase. The elastic modulus is related to the interatomic distance and bonding strength of atoms. The fracture strength and fracture strain increase with the densification of the coating. •The BSAS coating crystallizes at the test temperature.•Crystallization increases the elastic modulus of the BSAS coating.•The porosity of the coating decreases with increasing test temperatures.•The densification of the coating increases its fracture strength.