Synthesis and X-ray Crystal Structure of Meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene)

The pendant-arm macrocycle, meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene) has been synthesized and its single crystal structure determined. The molecule crystallizes in a primitive monoclinic cell, with the space group P21/a (#14). The cell dimensions...

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Bibliographic Details
Published in:Molecules (Basel, Switzerland) Switzerland), 2003-02, Vol.8 (2), p.243-250
Main Authors: Haines, Robert I., Hutchings, Dean R.
Format: Article
Language:English
Subjects:
1-methylnaphthalene
Crystal structure
Pendant-arm macrocycle
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Summary:The pendant-arm macrocycle, meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-di-(1-methylnaphthalene) has been synthesized and its single crystal structure determined. The molecule crystallizes in a primitive monoclinic cell, with the space group P21/a (#14). The cell dimensions are a = 10.778(3)Å, b = 13.809(3) Å, c = 11.420(2) Å, = 102.49(2)°, volume = 1659.5(6) Å3.
ISSN:1420-3049
1420-3049
DOI:10.3390/80200243