Loading…

A comprehensive strategy for exploring corrosion in iron-based artefacts through advanced Multiscale X-ray Microscopy

The best strategy to tackle complexity when analyzing corrosion in iron artefacts is to combine different analytical methods. Traditional techniques provide effective means to identify the chemistry and mineralogy of corrosion products. Nevertheless, a further step is necessary to upgrade the unders...

Full description

Saved in:
Bibliographic Details
Published in:Scientific reports 2022-04, Vol.12 (1), p.6125-6125, Article 6125
Main Authors: Bernabale, Martina, Cognigni, Flavio, Nigro, Lorenzo, Rossi, Marco, de Caro, Tilde, De Vito, Caterina
Format: Article
Language:English
Subjects:
Citations: Items that this one cites
Items that cite this one
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
cited_by cdi_FETCH-LOGICAL-c455w-d0a08ab85150b3a779ef36309704e8129a45f0d155b1250ba042292427db192b3
cites cdi_FETCH-LOGICAL-c455w-d0a08ab85150b3a779ef36309704e8129a45f0d155b1250ba042292427db192b3
container_end_page 6125
container_issue 1
container_start_page 6125
container_title Scientific reports
container_volume 12
creator Bernabale, Martina
Cognigni, Flavio
Nigro, Lorenzo
Rossi, Marco
de Caro, Tilde
De Vito, Caterina
description The best strategy to tackle complexity when analyzing corrosion in iron artefacts is to combine different analytical methods. Traditional techniques provide effective means to identify the chemistry and mineralogy of corrosion products. Nevertheless, a further step is necessary to upgrade the understanding of the corrosion evolution in three dimensions. In this regard, Multiscale X-ray Microscopy (XRM) enables multi-length scale visualization of the whole object and provides the spatial distribution of corrosion phases. Herein, we propose an integrated workflow to explore corrosion mechanisms in an iron-nail from Motya (Italy) through destructive and non-destructive techniques, which permit the extraction of the maximum information with the minimum sampling. The results reveal the internal structure of the artefact and the structural discontinuities which lead the corrosion, highlighting the compositional differences between the tip and the head of the iron nail.
doi_str_mv 10.1038/s41598-022-10151-w
format article
fullrecord <record><control><sourceid>proquest_doaj_</sourceid><recordid>TN_cdi_doaj_primary_oai_doaj_org_article_8e12735fae18458b815478e3a29fdb93</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><doaj_id>oai_doaj_org_article_8e12735fae18458b815478e3a29fdb93</doaj_id><sourcerecordid>2649996886</sourcerecordid><originalsourceid>FETCH-LOGICAL-c455w-d0a08ab85150b3a779ef36309704e8129a45f0d155b1250ba042292427db192b3</originalsourceid><addsrcrecordid>eNp9ks1u1DAUhSMEolXpC7BAltiwSfFvYm-QqqrQSq3YgMTOukluMh5l4mAnM8zb45mU0rLAsmTL_u6xfXyy7C2jF4wK_TFKpozOKec5o0yxfPciO-VUqpwLzl8-mZ9k5zGuaWqKG8nM6-xEKMlkoYvTbL4ktd-MAVc4RLdFEqcAE3Z70vpA8NfY--CGLkEh-Oj8QFzqwQ95BREbAmHCFuopkmkV_NytCDRbGOq0dT_3k4s19Eh-5AH25N7VSaP24_5N9qqFPuL5w3iWff98_e3qJr_7-uX26vIur6VSu7yhQDVUWjFFKwFlabAVhaCmpBI14wakamnDlKoYTwhQybnhkpdNxQyvxFl2u-g2HtZ2DG4DYW89OHtc8KGz6QGu7tFqZLwUqgVkWipdaaZkqVEAN21TGZG0Pi1a41xtsKlxSE71z0Sf7wxuZTu_tSYZr6RJAh8eBIL_OWOc7CbZg30PA_o5Wl5IY0yhdZHQ9_-gaz-HIVl1pGT6Vc4TxRfqYGsM2D5ehlF7CIldQmJTSOwxJHaXit49fcZjyZ9IJEAsQBwPP4_h79n_kf0Na67IzQ</addsrcrecordid><sourcetype>Open Website</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2649432222</pqid></control><display><type>article</type><title>A comprehensive strategy for exploring corrosion in iron-based artefacts through advanced Multiscale X-ray Microscopy</title><source>Open Access: PubMed Central</source><source>Publicly Available Content (ProQuest)</source><source>Free Full-Text Journals in Chemistry</source><source>Springer Nature - nature.com Journals - Fully Open Access</source><creator>Bernabale, Martina ; Cognigni, Flavio ; Nigro, Lorenzo ; Rossi, Marco ; de Caro, Tilde ; De Vito, Caterina</creator><creatorcontrib>Bernabale, Martina ; Cognigni, Flavio ; Nigro, Lorenzo ; Rossi, Marco ; de Caro, Tilde ; De Vito, Caterina</creatorcontrib><description>The best strategy to tackle complexity when analyzing corrosion in iron artefacts is to combine different analytical methods. Traditional techniques provide effective means to identify the chemistry and mineralogy of corrosion products. Nevertheless, a further step is necessary to upgrade the understanding of the corrosion evolution in three dimensions. In this regard, Multiscale X-ray Microscopy (XRM) enables multi-length scale visualization of the whole object and provides the spatial distribution of corrosion phases. Herein, we propose an integrated workflow to explore corrosion mechanisms in an iron-nail from Motya (Italy) through destructive and non-destructive techniques, which permit the extraction of the maximum information with the minimum sampling. The results reveal the internal structure of the artefact and the structural discontinuities which lead the corrosion, highlighting the compositional differences between the tip and the head of the iron nail.</description><identifier>ISSN: 2045-2322</identifier><identifier>EISSN: 2045-2322</identifier><identifier>DOI: 10.1038/s41598-022-10151-w</identifier><identifier>PMID: 35414686</identifier><language>eng</language><publisher>London: Nature Publishing Group UK</publisher><subject>639/166 ; 639/301 ; 639/638 ; 639/766 ; 639/925 ; Corrosion ; Humanities and Social Sciences ; Iron ; Iron - chemistry ; Microscopy ; Mineralogy ; multidisciplinary ; Science ; Science (multidisciplinary) ; Spatial distribution ; X-Rays</subject><ispartof>Scientific reports, 2022-04, Vol.12 (1), p.6125-6125, Article 6125</ispartof><rights>The Author(s) 2022</rights><rights>2022. The Author(s).</rights><rights>The Author(s) 2022. This work is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c455w-d0a08ab85150b3a779ef36309704e8129a45f0d155b1250ba042292427db192b3</citedby><cites>FETCH-LOGICAL-c455w-d0a08ab85150b3a779ef36309704e8129a45f0d155b1250ba042292427db192b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.proquest.com/docview/2649432222/fulltextPDF?pq-origsite=primo$$EPDF$$P50$$Gproquest$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.proquest.com/docview/2649432222?pq-origsite=primo$$EHTML$$P50$$Gproquest$$Hfree_for_read</linktohtml><link.rule.ids>230,314,727,780,784,885,25753,27924,27925,37012,37013,44590,53791,53793,75126</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/35414686$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Bernabale, Martina</creatorcontrib><creatorcontrib>Cognigni, Flavio</creatorcontrib><creatorcontrib>Nigro, Lorenzo</creatorcontrib><creatorcontrib>Rossi, Marco</creatorcontrib><creatorcontrib>de Caro, Tilde</creatorcontrib><creatorcontrib>De Vito, Caterina</creatorcontrib><title>A comprehensive strategy for exploring corrosion in iron-based artefacts through advanced Multiscale X-ray Microscopy</title><title>Scientific reports</title><addtitle>Sci Rep</addtitle><addtitle>Sci Rep</addtitle><description>The best strategy to tackle complexity when analyzing corrosion in iron artefacts is to combine different analytical methods. Traditional techniques provide effective means to identify the chemistry and mineralogy of corrosion products. Nevertheless, a further step is necessary to upgrade the understanding of the corrosion evolution in three dimensions. In this regard, Multiscale X-ray Microscopy (XRM) enables multi-length scale visualization of the whole object and provides the spatial distribution of corrosion phases. Herein, we propose an integrated workflow to explore corrosion mechanisms in an iron-nail from Motya (Italy) through destructive and non-destructive techniques, which permit the extraction of the maximum information with the minimum sampling. The results reveal the internal structure of the artefact and the structural discontinuities which lead the corrosion, highlighting the compositional differences between the tip and the head of the iron nail.</description><subject>639/166</subject><subject>639/301</subject><subject>639/638</subject><subject>639/766</subject><subject>639/925</subject><subject>Corrosion</subject><subject>Humanities and Social Sciences</subject><subject>Iron</subject><subject>Iron - chemistry</subject><subject>Microscopy</subject><subject>Mineralogy</subject><subject>multidisciplinary</subject><subject>Science</subject><subject>Science (multidisciplinary)</subject><subject>Spatial distribution</subject><subject>X-Rays</subject><issn>2045-2322</issn><issn>2045-2322</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><sourceid>PIMPY</sourceid><sourceid>DOA</sourceid><recordid>eNp9ks1u1DAUhSMEolXpC7BAltiwSfFvYm-QqqrQSq3YgMTOukluMh5l4mAnM8zb45mU0rLAsmTL_u6xfXyy7C2jF4wK_TFKpozOKec5o0yxfPciO-VUqpwLzl8-mZ9k5zGuaWqKG8nM6-xEKMlkoYvTbL4ktd-MAVc4RLdFEqcAE3Z70vpA8NfY--CGLkEh-Oj8QFzqwQ95BREbAmHCFuopkmkV_NytCDRbGOq0dT_3k4s19Eh-5AH25N7VSaP24_5N9qqFPuL5w3iWff98_e3qJr_7-uX26vIur6VSu7yhQDVUWjFFKwFlabAVhaCmpBI14wakamnDlKoYTwhQybnhkpdNxQyvxFl2u-g2HtZ2DG4DYW89OHtc8KGz6QGu7tFqZLwUqgVkWipdaaZkqVEAN21TGZG0Pi1a41xtsKlxSE71z0Sf7wxuZTu_tSYZr6RJAh8eBIL_OWOc7CbZg30PA_o5Wl5IY0yhdZHQ9_-gaz-HIVl1pGT6Vc4TxRfqYGsM2D5ehlF7CIldQmJTSOwxJHaXit49fcZjyZ9IJEAsQBwPP4_h79n_kf0Na67IzQ</recordid><startdate>20220412</startdate><enddate>20220412</enddate><creator>Bernabale, Martina</creator><creator>Cognigni, Flavio</creator><creator>Nigro, Lorenzo</creator><creator>Rossi, Marco</creator><creator>de Caro, Tilde</creator><creator>De Vito, Caterina</creator><general>Nature Publishing Group UK</general><general>Nature Publishing Group</general><general>Nature Portfolio</general><scope>C6C</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7X7</scope><scope>7XB</scope><scope>88A</scope><scope>88E</scope><scope>88I</scope><scope>8FE</scope><scope>8FH</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BBNVY</scope><scope>BENPR</scope><scope>BHPHI</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>K9.</scope><scope>LK8</scope><scope>M0S</scope><scope>M1P</scope><scope>M2P</scope><scope>M7P</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>Q9U</scope><scope>7X8</scope><scope>5PM</scope><scope>DOA</scope></search><sort><creationdate>20220412</creationdate><title>A comprehensive strategy for exploring corrosion in iron-based artefacts through advanced Multiscale X-ray Microscopy</title><author>Bernabale, Martina ; Cognigni, Flavio ; Nigro, Lorenzo ; Rossi, Marco ; de Caro, Tilde ; De Vito, Caterina</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c455w-d0a08ab85150b3a779ef36309704e8129a45f0d155b1250ba042292427db192b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>639/166</topic><topic>639/301</topic><topic>639/638</topic><topic>639/766</topic><topic>639/925</topic><topic>Corrosion</topic><topic>Humanities and Social Sciences</topic><topic>Iron</topic><topic>Iron - chemistry</topic><topic>Microscopy</topic><topic>Mineralogy</topic><topic>multidisciplinary</topic><topic>Science</topic><topic>Science (multidisciplinary)</topic><topic>Spatial distribution</topic><topic>X-Rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bernabale, Martina</creatorcontrib><creatorcontrib>Cognigni, Flavio</creatorcontrib><creatorcontrib>Nigro, Lorenzo</creatorcontrib><creatorcontrib>Rossi, Marco</creatorcontrib><creatorcontrib>de Caro, Tilde</creatorcontrib><creatorcontrib>De Vito, Caterina</creatorcontrib><collection>Springer Nature OA Free Journals</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Health &amp; Medical Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Biology Database (Alumni Edition)</collection><collection>Medical Database (Alumni Edition)</collection><collection>Science Database (Alumni Edition)</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Natural Science Collection</collection><collection>Hospital Premium Collection</collection><collection>Hospital Premium Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>ProQuest Central (Alumni)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>Biological Science Collection</collection><collection>ProQuest Central</collection><collection>Natural Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>Health Research Premium Collection</collection><collection>Health Research Premium Collection (Alumni)</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Health &amp; Medical Complete (Alumni)</collection><collection>ProQuest Biological Science Collection</collection><collection>Health &amp; Medical Collection (Alumni Edition)</collection><collection>Medical Database</collection><collection>Science Database</collection><collection>Biological Science Database</collection><collection>Publicly Available Content (ProQuest)</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central Basic</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>Scientific reports</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bernabale, Martina</au><au>Cognigni, Flavio</au><au>Nigro, Lorenzo</au><au>Rossi, Marco</au><au>de Caro, Tilde</au><au>De Vito, Caterina</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A comprehensive strategy for exploring corrosion in iron-based artefacts through advanced Multiscale X-ray Microscopy</atitle><jtitle>Scientific reports</jtitle><stitle>Sci Rep</stitle><addtitle>Sci Rep</addtitle><date>2022-04-12</date><risdate>2022</risdate><volume>12</volume><issue>1</issue><spage>6125</spage><epage>6125</epage><pages>6125-6125</pages><artnum>6125</artnum><issn>2045-2322</issn><eissn>2045-2322</eissn><abstract>The best strategy to tackle complexity when analyzing corrosion in iron artefacts is to combine different analytical methods. Traditional techniques provide effective means to identify the chemistry and mineralogy of corrosion products. Nevertheless, a further step is necessary to upgrade the understanding of the corrosion evolution in three dimensions. In this regard, Multiscale X-ray Microscopy (XRM) enables multi-length scale visualization of the whole object and provides the spatial distribution of corrosion phases. Herein, we propose an integrated workflow to explore corrosion mechanisms in an iron-nail from Motya (Italy) through destructive and non-destructive techniques, which permit the extraction of the maximum information with the minimum sampling. The results reveal the internal structure of the artefact and the structural discontinuities which lead the corrosion, highlighting the compositional differences between the tip and the head of the iron nail.</abstract><cop>London</cop><pub>Nature Publishing Group UK</pub><pmid>35414686</pmid><doi>10.1038/s41598-022-10151-w</doi><tpages>1</tpages><oa>free_for_read</oa></addata></record>
fulltext fulltext
identifier ISSN: 2045-2322
ispartof Scientific reports, 2022-04, Vol.12 (1), p.6125-6125, Article 6125
issn 2045-2322
2045-2322
language eng
recordid cdi_doaj_primary_oai_doaj_org_article_8e12735fae18458b815478e3a29fdb93
source Open Access: PubMed Central; Publicly Available Content (ProQuest); Free Full-Text Journals in Chemistry; Springer Nature - nature.com Journals - Fully Open Access
subjects 639/166
639/301
639/638
639/766
639/925
Corrosion
Humanities and Social Sciences
Iron
Iron - chemistry
Microscopy
Mineralogy
multidisciplinary
Science
Science (multidisciplinary)
Spatial distribution
X-Rays
title A comprehensive strategy for exploring corrosion in iron-based artefacts through advanced Multiscale X-ray Microscopy
url http://sfxeu10.hosted.exlibrisgroup.com/loughborough?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-25T16%3A40%3A49IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_doaj_&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=A%20comprehensive%20strategy%20for%20exploring%20corrosion%20in%20iron-based%20artefacts%20through%20advanced%20Multiscale%20X-ray%20Microscopy&rft.jtitle=Scientific%20reports&rft.au=Bernabale,%20Martina&rft.date=2022-04-12&rft.volume=12&rft.issue=1&rft.spage=6125&rft.epage=6125&rft.pages=6125-6125&rft.artnum=6125&rft.issn=2045-2322&rft.eissn=2045-2322&rft_id=info:doi/10.1038/s41598-022-10151-w&rft_dat=%3Cproquest_doaj_%3E2649996886%3C/proquest_doaj_%3E%3Cgrp_id%3Ecdi_FETCH-LOGICAL-c455w-d0a08ab85150b3a779ef36309704e8129a45f0d155b1250ba042292427db192b3%3C/grp_id%3E%3Coa%3E%3C/oa%3E%3Curl%3E%3C/url%3E&rft_id=info:oai/&rft_pqid=2649432222&rft_id=info:pmid/35414686&rfr_iscdi=true