An eco-compatible access to diversified bisoxazolone and bisimidazole derivatives

An efficient, straight-forward and eco-friendly synthetic strategy for the assembly of novel bisoxazolones via a four-component, sequential reaction of dialdehydes, glycine, benzoyl chloride and acetic anhydride, using ultrasound radiation, is described. Additionally, a diverse group of new bisimida...

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Published in:ARKIVOC free online journal of organic chemistry 2018-05, Vol.2018 (3), p.338-353
Main Authors: Arafa, Wael Abdelgayed Ahmed, Abdel-Magied, Ahmed Fawzy
Format: Article
Language:English
Subjects:
bis-imidazoles
Bisoxazolones
multi-component synthesis
solvent-free
ultrasound-assisted
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Abdel-Magied, Ahmed Fawzy
description An efficient, straight-forward and eco-friendly synthetic strategy for the assembly of novel bisoxazolones via a four-component, sequential reaction of dialdehydes, glycine, benzoyl chloride and acetic anhydride, using ultrasound radiation, is described. Additionally, a diverse group of new bisimidazoles has been synthesized in good yields by the sonication of diamines and (Z)-4-arylidene-2-phenyloxazol-5(4H)-ones. These approaches have resulted in a number of successful routes for the facile synthesis of bis-oxazolone and bis-imidazole frameworks within minutes of irradiation. Excellent outcomes using these environmentally-friendly parameters make these synthetic schemes ideal, sustainable, green-chemistry procedures and provide simple access towards the preparation of bisheterocycles. [GRAPHICS] .
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subjects bis-imidazoles
Bisoxazolones
multi-component synthesis
solvent-free
ultrasound-assisted
title An eco-compatible access to diversified bisoxazolone and bisimidazole derivatives
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