Microwave Synthesis of (4-hydroxy Phenyl) 3-oxo butanoate

The product 3 was previously prepared [1] using C6H6 in the presence of pyridine. A mixture of hydroquinone 1 (0.66 g, 6 mmol), ethyl acetoacetate 2 (0.78 g, 6 mmol) and monmorillonite K10 (0.43 g, 30 % by weight of the total reactants) [2,3] was placed in a pyrex tube which was then introduced into...

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Bibliographic Details
Published in:MolBank 2008-03, Vol.2008 (1), p.M561
Main Authors: Ramdani, Mohammed, Benchat, Nour-Eddine, Anaflous, Abderrahmane, El Kalai, Fouad
Format: Article
Language:English
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Summary:The product 3 was previously prepared [1] using C6H6 in the presence of pyridine. A mixture of hydroquinone 1 (0.66 g, 6 mmol), ethyl acetoacetate 2 (0.78 g, 6 mmol) and monmorillonite K10 (0.43 g, 30 % by weight of the total reactants) [2,3] was placed in a pyrex tube which was then introduced into a Maxidigest MX 350 Prolabo microwave monomode reactor fitted with a rotational system [4].
ISSN:1422-8599
1422-8599
DOI:10.3390/M561