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Redetermined structure of 4,4′-bipyridine–1,4-phenylenediacetic acid (1/1) co-crystal
The asymmetric unit of the title 1:1 co-crystal, C 10 H 8 N 2 ·C 10 H 10 O 4 , consists of one half-molecule each of 4,4′-bipyridine and 1,4-phenylenediacetic acid: the complete molecules are generated by crystallographic inversion centres. The dihedral angle between the –CO 2 H group and the benzen...
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| Published in: | Acta crystallographica. Section E, Crystallographic communications Crystallographic communications, 2015-10, Vol.71 (10), p.o799-o800 |
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| Main Authors: | , |
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| Language: | English |
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| container_end_page | o800 |
| container_issue | 10 |
| container_start_page | o799 |
| container_title | Acta crystallographica. Section E, Crystallographic communications |
| container_volume | 71 |
| creator | Paul, Rima Bora, Sanchay Jyoti |
| description | The asymmetric unit of the title 1:1 co-crystal, C
10
H
8
N
2
·C
10
H
10
O
4
, consists of one half-molecule each of 4,4′-bipyridine and 1,4-phenylenediacetic acid: the complete molecules are generated by crystallographic inversion centres. The dihedral angle between the –CO
2
H group and the benzene ring in the diacid is 73.02 (7)°. In the crystal, the components are linked by O—H...N hydrogen bonds, generating [1-2-1] chains of alternating amine and carboxylic acid molecules. The chains are cross-linked by C—H...O interactions. This structure was previously incorrectly described as a (C
10
H
10
N
2
)
2+
·(C
10
H
8
O
4
)
2−
molecular salt [Jia
et al.
(2009).
Acta Cryst.
E
65
, o2490–o2490]. |
| doi_str_mv | 10.1107/S2056989015017569 |
| format | article |
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10
H
8
N
2
·C
10
H
10
O
4
, consists of one half-molecule each of 4,4′-bipyridine and 1,4-phenylenediacetic acid: the complete molecules are generated by crystallographic inversion centres. The dihedral angle between the –CO
2
H group and the benzene ring in the diacid is 73.02 (7)°. In the crystal, the components are linked by O—H...N hydrogen bonds, generating [1-2-1] chains of alternating amine and carboxylic acid molecules. The chains are cross-linked by C—H...O interactions. This structure was previously incorrectly described as a (C
10
H
10
N
2
)
2+
·(C
10
H
8
O
4
)
2−
molecular salt [Jia
et al.
(2009).
Acta Cryst.
E
65
, o2490–o2490].</description><identifier>ISSN: 2056-9890</identifier><identifier>EISSN: 2056-9890</identifier><identifier>DOI: 10.1107/S2056989015017569</identifier><language>eng</language><publisher>International Union of Crystallography</publisher><subject>co-crystal ; crystal structure ; hydrogen bonding ; supramolecular interaction</subject><ispartof>Acta crystallographica. Section E, Crystallographic communications, 2015-10, Vol.71 (10), p.o799-o800</ispartof><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c306t-6c27fc1dab706bca0f9c08aafc23d3876dda31fa56084559bb3095560a05024b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Paul, Rima</creatorcontrib><creatorcontrib>Bora, Sanchay Jyoti</creatorcontrib><title>Redetermined structure of 4,4′-bipyridine–1,4-phenylenediacetic acid (1/1) co-crystal</title><title>Acta crystallographica. Section E, Crystallographic communications</title><description>The asymmetric unit of the title 1:1 co-crystal, C
10
H
8
N
2
·C
10
H
10
O
4
, consists of one half-molecule each of 4,4′-bipyridine and 1,4-phenylenediacetic acid: the complete molecules are generated by crystallographic inversion centres. The dihedral angle between the –CO
2
H group and the benzene ring in the diacid is 73.02 (7)°. In the crystal, the components are linked by O—H...N hydrogen bonds, generating [1-2-1] chains of alternating amine and carboxylic acid molecules. The chains are cross-linked by C—H...O interactions. This structure was previously incorrectly described as a (C
10
H
10
N
2
)
2+
·(C
10
H
8
O
4
)
2−
molecular salt [Jia
et al.
(2009).
Acta Cryst.
E
65
, o2490–o2490].</description><subject>co-crystal</subject><subject>crystal structure</subject><subject>hydrogen bonding</subject><subject>supramolecular interaction</subject><issn>2056-9890</issn><issn>2056-9890</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><sourceid>DOA</sourceid><recordid>eNplkM9Kw0AQxoMoWGofwFuOCo2dyWY3yVGKfwoFwT8HT2F2dqNb0qZs0kNufQffxEfqk5haEcHTfPPN8OPjC4JzhCtESCdPMUiVZzmgBEx7eRQM9la0947_6NNg1DQLAMBECiXjQfD6aI1trV-6lTVh0_oNtxtvw7oMk3Gy235G2q0770x_320_cJxE63e76irb_zti2zoOiZ0JL3CClyHXEfuuaak6C05Kqho7-pnD4OX25nl6H80f7mbT63nEAlQbKY7TktGQTkFpJihzhoyo5FgYkaXKGBJYklSQJVLmWgvIZb8RSIgTLYbB7MA1NS2KtXdL8l1Rkyu-jdq_FeT7lJUtdGyQKdZalTrRlGSMaPOcYlCYWcU9Cw8s9nXTeFv-8hCKfdXFv6rFF3hYcfU</recordid><startdate>20151001</startdate><enddate>20151001</enddate><creator>Paul, Rima</creator><creator>Bora, Sanchay Jyoti</creator><general>International Union of Crystallography</general><scope>AAYXX</scope><scope>CITATION</scope><scope>DOA</scope></search><sort><creationdate>20151001</creationdate><title>Redetermined structure of 4,4′-bipyridine–1,4-phenylenediacetic acid (1/1) co-crystal</title><author>Paul, Rima ; Bora, Sanchay Jyoti</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c306t-6c27fc1dab706bca0f9c08aafc23d3876dda31fa56084559bb3095560a05024b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>co-crystal</topic><topic>crystal structure</topic><topic>hydrogen bonding</topic><topic>supramolecular interaction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Paul, Rima</creatorcontrib><creatorcontrib>Bora, Sanchay Jyoti</creatorcontrib><collection>CrossRef</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>Acta crystallographica. Section E, Crystallographic communications</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Paul, Rima</au><au>Bora, Sanchay Jyoti</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Redetermined structure of 4,4′-bipyridine–1,4-phenylenediacetic acid (1/1) co-crystal</atitle><jtitle>Acta crystallographica. Section E, Crystallographic communications</jtitle><date>2015-10-01</date><risdate>2015</risdate><volume>71</volume><issue>10</issue><spage>o799</spage><epage>o800</epage><pages>o799-o800</pages><issn>2056-9890</issn><eissn>2056-9890</eissn><abstract>The asymmetric unit of the title 1:1 co-crystal, C
10
H
8
N
2
·C
10
H
10
O
4
, consists of one half-molecule each of 4,4′-bipyridine and 1,4-phenylenediacetic acid: the complete molecules are generated by crystallographic inversion centres. The dihedral angle between the –CO
2
H group and the benzene ring in the diacid is 73.02 (7)°. In the crystal, the components are linked by O—H...N hydrogen bonds, generating [1-2-1] chains of alternating amine and carboxylic acid molecules. The chains are cross-linked by C—H...O interactions. This structure was previously incorrectly described as a (C
10
H
10
N
2
)
2+
·(C
10
H
8
O
4
)
2−
molecular salt [Jia
et al.
(2009).
Acta Cryst.
E
65
, o2490–o2490].</abstract><pub>International Union of Crystallography</pub><doi>10.1107/S2056989015017569</doi><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 2056-9890 |
| ispartof | Acta crystallographica. Section E, Crystallographic communications, 2015-10, Vol.71 (10), p.o799-o800 |
| issn | 2056-9890 2056-9890 |
| language | eng |
| recordid | cdi_doaj_primary_oai_doaj_org_article_b2d1ca2bb6fb4ba48c11e99a20618e6c |
| source | Open Access: PubMed Central; IngentaConnect Journals |
| subjects | co-crystal crystal structure hydrogen bonding supramolecular interaction |
| title | Redetermined structure of 4,4′-bipyridine–1,4-phenylenediacetic acid (1/1) co-crystal |
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