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Application of the Sol-Gel Method at the Fabrication of PLZT:Yb3+ Ceramics
The aim of presented study was to obtain the PLZT:Yb ceramics. Nanopowders of itterbium doped PLZT materials were synthesized by the sol-gel method from high quality metaloorganic precursors, as lead (II) acetate, lanthanum acetate, ytterbium acetate, zirconium (IV) propoxide and titanium (IV) propo...
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| Published in: | Archives of metallurgy and materials 2016-09, Vol.61 (3), p.1095-1100 |
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| cited_by | cdi_FETCH-LOGICAL-c406t-4132b2d23aac3c6ad039d5687157d3c63e6bf8d3ec2e1c9cda4c44e475a43fd03 |
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| container_title | Archives of metallurgy and materials |
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| creator | Osińska, K. Płońska, M. Marzec, A. |
| description | The aim of presented study was to obtain the PLZT:Yb
ceramics. Nanopowders of itterbium doped PLZT materials were synthesized by the sol-gel method from high quality metaloorganic precursors, as lead (II) acetate, lanthanum acetate, ytterbium acetate, zirconium (IV) propoxide and titanium (IV) propoxide. Anhydrous acetic acid and n-propyl alcohol were used as solvents, while acetyloacetone was added as stabilizer of hydrolysis reactions. Thermal evolution of the dried gels, before and after calcination, was studied by the simultaneous thermal analysis. The amorphous PLZT:Yb
gels were first calcined in the furnace at
= 850°C, and then mixed in the planetary ball mill. Additionally, the mean particle sizes were calculated by means of powder specific surface area measurements, based on the BET physical adsorption isotherm. Such obtained powders were subsequently pressed into pellets, and sintered by the free sintering method at temperature
= 1250°C / 6h. The morphology of fabricated PLZT:Yb
ceramic powders and samples was studied using Scanning Electron Microscopy. Chemical characterization of samples was carried on using the Energy-dispersive X-ray spectroscopy - EDS system. Studies provided detailed data concerning the relationships between doping and preparing conditions on the basic physical and chemical properties of obtained ceramic materials. |
| doi_str_mv | 10.1515/amm-2016-0236 |
| format | article |
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ceramics. Nanopowders of itterbium doped PLZT materials were synthesized by the sol-gel method from high quality metaloorganic precursors, as lead (II) acetate, lanthanum acetate, ytterbium acetate, zirconium (IV) propoxide and titanium (IV) propoxide. Anhydrous acetic acid and n-propyl alcohol were used as solvents, while acetyloacetone was added as stabilizer of hydrolysis reactions. Thermal evolution of the dried gels, before and after calcination, was studied by the simultaneous thermal analysis. The amorphous PLZT:Yb
gels were first calcined in the furnace at
= 850°C, and then mixed in the planetary ball mill. Additionally, the mean particle sizes were calculated by means of powder specific surface area measurements, based on the BET physical adsorption isotherm. Such obtained powders were subsequently pressed into pellets, and sintered by the free sintering method at temperature
= 1250°C / 6h. The morphology of fabricated PLZT:Yb
ceramic powders and samples was studied using Scanning Electron Microscopy. Chemical characterization of samples was carried on using the Energy-dispersive X-ray spectroscopy - EDS system. Studies provided detailed data concerning the relationships between doping and preparing conditions on the basic physical and chemical properties of obtained ceramic materials.</description><identifier>ISSN: 2300-1909</identifier><identifier>ISSN: 1733-3490</identifier><identifier>EISSN: 2300-1909</identifier><identifier>DOI: 10.1515/amm-2016-0236</identifier><language>eng</language><publisher>Warsaw: De Gruyter Open</publisher><subject>Acetic acid ; Adsorption ; Ceramic powders ; Ceramics ; Chemical properties ; Crystal structure ; Gels ; Lanthanum ; Lead ; Lead lanthanum zirconate titanate ; Morphology ; perovskite structure ceramics ; Planetary evolution ; PLZT:Yb ; PLZT:Yb3+ ceramics ; Roasting ; Sintering (powder metallurgy) ; sol-gel method ; Sol-gel processes ; Thermal analysis ; Thermal evolution ; Titanium ; Ytterbium ; Ytterbium acetate ; Zirconium</subject><ispartof>Archives of metallurgy and materials, 2016-09, Vol.61 (3), p.1095-1100</ispartof><rights>Copyright De Gruyter Open Sp. z o.o. 2016</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c406t-4132b2d23aac3c6ad039d5687157d3c63e6bf8d3ec2e1c9cda4c44e475a43fd03</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.proquest.com/docview/1833194395?pq-origsite=primo$$EHTML$$P50$$Gproquest$$Hfree_for_read</linktohtml><link.rule.ids>314,780,784,25753,27924,27925,37012,44590</link.rule.ids></links><search><creatorcontrib>Osińska, K.</creatorcontrib><creatorcontrib>Płońska, M.</creatorcontrib><creatorcontrib>Marzec, A.</creatorcontrib><title>Application of the Sol-Gel Method at the Fabrication of PLZT:Yb3+ Ceramics</title><title>Archives of metallurgy and materials</title><description>The aim of presented study was to obtain the PLZT:Yb
ceramics. Nanopowders of itterbium doped PLZT materials were synthesized by the sol-gel method from high quality metaloorganic precursors, as lead (II) acetate, lanthanum acetate, ytterbium acetate, zirconium (IV) propoxide and titanium (IV) propoxide. Anhydrous acetic acid and n-propyl alcohol were used as solvents, while acetyloacetone was added as stabilizer of hydrolysis reactions. Thermal evolution of the dried gels, before and after calcination, was studied by the simultaneous thermal analysis. The amorphous PLZT:Yb
gels were first calcined in the furnace at
= 850°C, and then mixed in the planetary ball mill. Additionally, the mean particle sizes were calculated by means of powder specific surface area measurements, based on the BET physical adsorption isotherm. Such obtained powders were subsequently pressed into pellets, and sintered by the free sintering method at temperature
= 1250°C / 6h. The morphology of fabricated PLZT:Yb
ceramic powders and samples was studied using Scanning Electron Microscopy. Chemical characterization of samples was carried on using the Energy-dispersive X-ray spectroscopy - EDS system. Studies provided detailed data concerning the relationships between doping and preparing conditions on the basic physical and chemical properties of obtained ceramic materials.</description><subject>Acetic acid</subject><subject>Adsorption</subject><subject>Ceramic powders</subject><subject>Ceramics</subject><subject>Chemical properties</subject><subject>Crystal structure</subject><subject>Gels</subject><subject>Lanthanum</subject><subject>Lead</subject><subject>Lead lanthanum zirconate titanate</subject><subject>Morphology</subject><subject>perovskite structure ceramics</subject><subject>Planetary evolution</subject><subject>PLZT:Yb</subject><subject>PLZT:Yb3+ ceramics</subject><subject>Roasting</subject><subject>Sintering (powder metallurgy)</subject><subject>sol-gel method</subject><subject>Sol-gel processes</subject><subject>Thermal analysis</subject><subject>Thermal evolution</subject><subject>Titanium</subject><subject>Ytterbium</subject><subject>Ytterbium acetate</subject><subject>Zirconium</subject><issn>2300-1909</issn><issn>1733-3490</issn><issn>2300-1909</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><sourceid>PIMPY</sourceid><sourceid>DOA</sourceid><recordid>eNqlkMFLwzAUh4soOHRH7wWPUs1r0nYRL2O4OZkoOA96CWnyunV0S00zZP-96SqygzdzyePxvd97fEFwAeQaEkhu5HodxQTSiMQ0PQp6MSUkAk748UF9GvSbZkX8ywgDYL3gcVjXVamkK80mNEXolhi-miqaYBU-oVsaHUq3745lbg_Al9nH_PY9p1fhCK1cl6o5D04KWTXY__nPgrfx_Xz0EM2eJ9PRcBYpRlIXMaBxHuuYSqmoSqUmlOskHWSQZNo3KKZ5MdAUVYyguNKSKcaQZYlktPD0WTDtcrWRK1Hbci3tThhZin3D2IWQ1pWqQpEXmMWaac2SjCUAPEPGOSEIhdcEic-67LJqaz632DixMlu78ecLGFAKnFHeUlFHKWuaxmLxuxWIaO0Lb1-09kVr3_N3Hf8lK4dW48Jud744CP9rLgUKzOv5xzjx134DdE-bgg</recordid><startdate>20160901</startdate><enddate>20160901</enddate><creator>Osińska, K.</creator><creator>Płońska, M.</creator><creator>Marzec, A.</creator><general>De Gruyter Open</general><general>Polish Academy of Sciences</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>DOA</scope></search><sort><creationdate>20160901</creationdate><title>Application of the Sol-Gel Method at the Fabrication of PLZT:Yb3+ Ceramics</title><author>Osińska, K. ; Płońska, M. ; Marzec, A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c406t-4132b2d23aac3c6ad039d5687157d3c63e6bf8d3ec2e1c9cda4c44e475a43fd03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Acetic acid</topic><topic>Adsorption</topic><topic>Ceramic powders</topic><topic>Ceramics</topic><topic>Chemical properties</topic><topic>Crystal structure</topic><topic>Gels</topic><topic>Lanthanum</topic><topic>Lead</topic><topic>Lead lanthanum zirconate titanate</topic><topic>Morphology</topic><topic>perovskite structure ceramics</topic><topic>Planetary evolution</topic><topic>PLZT:Yb</topic><topic>PLZT:Yb3+ ceramics</topic><topic>Roasting</topic><topic>Sintering (powder metallurgy)</topic><topic>sol-gel method</topic><topic>Sol-gel processes</topic><topic>Thermal analysis</topic><topic>Thermal evolution</topic><topic>Titanium</topic><topic>Ytterbium</topic><topic>Ytterbium acetate</topic><topic>Zirconium</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Osińska, K.</creatorcontrib><creatorcontrib>Płońska, M.</creatorcontrib><creatorcontrib>Marzec, A.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Access via ProQuest (Open Access)</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>Archives of metallurgy and materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Osińska, K.</au><au>Płońska, M.</au><au>Marzec, A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Application of the Sol-Gel Method at the Fabrication of PLZT:Yb3+ Ceramics</atitle><jtitle>Archives of metallurgy and materials</jtitle><date>2016-09-01</date><risdate>2016</risdate><volume>61</volume><issue>3</issue><spage>1095</spage><epage>1100</epage><pages>1095-1100</pages><issn>2300-1909</issn><issn>1733-3490</issn><eissn>2300-1909</eissn><abstract>The aim of presented study was to obtain the PLZT:Yb
ceramics. Nanopowders of itterbium doped PLZT materials were synthesized by the sol-gel method from high quality metaloorganic precursors, as lead (II) acetate, lanthanum acetate, ytterbium acetate, zirconium (IV) propoxide and titanium (IV) propoxide. Anhydrous acetic acid and n-propyl alcohol were used as solvents, while acetyloacetone was added as stabilizer of hydrolysis reactions. Thermal evolution of the dried gels, before and after calcination, was studied by the simultaneous thermal analysis. The amorphous PLZT:Yb
gels were first calcined in the furnace at
= 850°C, and then mixed in the planetary ball mill. Additionally, the mean particle sizes were calculated by means of powder specific surface area measurements, based on the BET physical adsorption isotherm. Such obtained powders were subsequently pressed into pellets, and sintered by the free sintering method at temperature
= 1250°C / 6h. The morphology of fabricated PLZT:Yb
ceramic powders and samples was studied using Scanning Electron Microscopy. Chemical characterization of samples was carried on using the Energy-dispersive X-ray spectroscopy - EDS system. Studies provided detailed data concerning the relationships between doping and preparing conditions on the basic physical and chemical properties of obtained ceramic materials.</abstract><cop>Warsaw</cop><pub>De Gruyter Open</pub><doi>10.1515/amm-2016-0236</doi><tpages>6</tpages><oa>free_for_read</oa></addata></record> |
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| ispartof | Archives of metallurgy and materials, 2016-09, Vol.61 (3), p.1095-1100 |
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| source | Access via ProQuest (Open Access); IngentaConnect Journals |
| subjects | Acetic acid Adsorption Ceramic powders Ceramics Chemical properties Crystal structure Gels Lanthanum Lead Lead lanthanum zirconate titanate Morphology perovskite structure ceramics Planetary evolution PLZT:Yb PLZT:Yb3+ ceramics Roasting Sintering (powder metallurgy) sol-gel method Sol-gel processes Thermal analysis Thermal evolution Titanium Ytterbium Ytterbium acetate Zirconium |
| title | Application of the Sol-Gel Method at the Fabrication of PLZT:Yb3+ Ceramics |
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