3-[N-(4-Methoxybenzyl)amino]benzo[de]anthracen-7-one

Herein, we describe the synthesis of 3-[N-(4-methoxybenzyl)amino]benzo[de]anthracen-7-one via a two-step procedure including 3-aminobenzanthrone condensation with anisaldehyde and following reduction of obtained imine to appropriate amine by sodium borohydride. The structure of the synthesized compo...

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Bibliographic Details
Published in:MolBank 2021-12, Vol.2021 (4), p.M1287
Main Authors: Kirilova, Alise, Pučkins, Aleksandrs, Belyakov, Sergey, Kirilova, Elena
Format: Article
Language:English
Subjects:
3-aminobenzanthrone
azomethine
Chemical analysis
Crystal structure
Fluorescence
fluorescent dye
Gravimetric analysis
Hydrocarbons
Infrared analysis
Infrared spectroscopy
Mass spectrometry
NMR spectroscopy
Organic chemistry
reduction
secondary amine
Single crystals
Solvents
Spectroscopic analysis
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Summary:Herein, we describe the synthesis of 3-[N-(4-methoxybenzyl)amino]benzo[de]anthracen-7-one via a two-step procedure including 3-aminobenzanthrone condensation with anisaldehyde and following reduction of obtained imine to appropriate amine by sodium borohydride. The structure of the synthesized compounds was established by elemental analysis, nuclear magnetic resonance spectroscopy, mass spectrometry (EI-MS), and infrared spectroscopy (FT-IR) and confirmed by single-crystal X-ray diffraction. The title compound was analyzed by thermal gravimetric analysis, UV/vis, and fluorescence spectroscopy.
ISSN:1422-8599
1422-8599
DOI:10.3390/M1287