Extraction with SPME and synthesis of 2-methyl-6-vinylpyrazine by a 'one pot' reaction using microwaves

A synthesis of 2-methyl-6-vinylpyrazine was carried out by way of a 'one pot' reaction. In order to establish the efficiency of this synthesis the extraction of the volatiles released by male papaya fruit flies was performed by SPME (solid phase micro-extraction). The compound was separate...

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Bibliographic Details
Published in:Molecules (Basel, Switzerland) Switzerland), 2009-06, Vol.14 (6), p.2160-2166
Main Authors: Robledo, Norma, Escalante, Jaime, Arzuffi, René
Format: Article
Language:English
Subjects:
2-methyl-6-vinylpyrazine
Animals
Benzenesulfonates - chemistry
Charcoal
Chromatography
Gas Chromatography-Mass Spectrometry
Hoffman methylation
Magnetic Resonance Spectroscopy
Male
Males
Mass spectrometry
microwave
Microwaves
Molecular Structure
Pheromones
Pyrazines - chemical synthesis
Pyrazines - chemistry
Pyrazines - isolation & purification
Scientific imaging
sexual pheromone
SPME
Tephritidae - chemistry
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Summary:A synthesis of 2-methyl-6-vinylpyrazine was carried out by way of a 'one pot' reaction. In order to establish the efficiency of this synthesis the extraction of the volatiles released by male papaya fruit flies was performed by SPME (solid phase micro-extraction). The compound was separated and identified using GC/MSD (gas chromatography/mass spectrometry detector).
ISSN:1420-3049
1420-3049
DOI:10.3390/molecules14062160