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Novel Protocol for Synthesis of O,O-Dialkyl Monothiophospharic Acid Sodium Salt
Preparation of O,O-dialkyl monothiophospharic acid sodium salt (DMP-SNa) by addition of sulphur selectively on phosphorous using organic base to form a salt of O,O-dialkyl monothiophospharic acid trialkyl amine salt which is soluble in the non-polar organic solvent and treated with alkali to form O,...
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Published in: | Orbital : The Electronic Journal of Chemistry 2021-12, Vol.13 (5) |
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Main Authors: | , , |
Format: | Article |
Language: | English |
Subjects: | |
Online Access: | Get full text |
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Summary: | Preparation of O,O-dialkyl monothiophospharic acid sodium salt (DMP-SNa) by addition of sulphur selectively on phosphorous using organic base to form a salt of O,O-dialkyl monothiophospharic acid trialkyl amine salt which is soluble in the non-polar organic solvent and treated with alkali to form O,O-dialkyl monothiophospharic acid sodium salt (DAP-SNa). Trialkylamine becomes free and remains in the nonpolar solvents can be recycled. This synthesis method is effluent free. DOI: http://dx.doi.org/10.17807/orbital.v13i5.1597 |
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ISSN: | 1984-6428 |