The Use of Nuclear Magnetic Resonance Spectroscopy (NMR) to Characterize Bitumen Used in the Road Pavements Industry: A Review

Bitumen, a vital component in road pavement construction, exhibits complex chemo-mechanical properties that necessitate thorough characterization for enhanced understanding and potential modifications. Nuclear Magnetic Resonance (NMR) spectroscopy emerges as a valuable technique for probing the stru...

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Published in:Molecules (Basel, Switzerland) Switzerland), 2024-08, Vol.29 (17), p.4038
Main Authors: Shaikhah, Dilshad, Oliviero Rossi, Cesare, Luca, Giuseppina De, Angelico, Ruggero, Calandra, Pietro, Caputo, Paolino
Format: Article
Language:English
Subjects:
Aggregates
Asphalt pavements
bitumen
Colloids
Crude oil
Molecular weight
NMR
Nuclear magnetic resonance
Nuclear Magnetic Resonance Spectroscopy (NMR)
Physical Chemical Characterization
Resins
Roads & highways
Temperature
Water damage
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container_start_page 4038
container_title Molecules (Basel, Switzerland)
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creator Shaikhah, Dilshad
Oliviero Rossi, Cesare
Luca, Giuseppina De
Angelico, Ruggero
Calandra, Pietro
Caputo, Paolino
description Bitumen, a vital component in road pavement construction, exhibits complex chemo-mechanical properties that necessitate thorough characterization for enhanced understanding and potential modifications. Nuclear Magnetic Resonance (NMR) spectroscopy emerges as a valuable technique for probing the structural and compositional features of bitumen. This review presents an in-depth exploration of the role of NMR spectroscopy in bitumen characterization, highlighting its diverse applications in determining bitumen content, group composition, molecular dynamics, and interaction with additives. Various NMR techniques, including free induction decay (FID), Carr-Purcell-Meilboom-Gill (CPMG), and Pulsed Field Gradient Stimulated Echo (PFGSE), are discussed in the context of their utility in bitumen analysis. Case studies, challenges, and limitations associated with NMR-based bitumen characterization are critically evaluated, offering insights into potential future research directions. Overall, this review provides a comprehensive overview of the current state-of-the-art in NMR-based bitumen characterization and identifies avenues for further advancement in the field.
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subjects Aggregates
Asphalt pavements
bitumen
Colloids
Crude oil
Molecular weight
NMR
Nuclear magnetic resonance
Nuclear Magnetic Resonance Spectroscopy (NMR)
Physical Chemical Characterization
Resins
Roads & highways
Temperature
Water damage
title The Use of Nuclear Magnetic Resonance Spectroscopy (NMR) to Characterize Bitumen Used in the Road Pavements Industry: A Review
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