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Aquabis[ N ′-(1,3-dithiolan-2-ylidene)-2-hydroxybenzohydrazidato(0.5−)-κ 2 N ′, O ]sodium(I)
The title compound, [Na(C 10 H 9.5 N 2 O 2 S 2 ) 2 (H 2 O)], is a molecular sodium complex with N ′-(1,3-dithiolan-2-yl)-2-hydroxybenzohydrazide ligands with the negative charge spread evenly over both, and a water molecule. The Na I ion coordination is distorted trigonal–bipyramidal, formed by two...
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| Published in: | Acta crystallographica. Section E, Structure reports online Structure reports online, 2012-06, Vol.68 (6), p.m827-m828 |
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| Main Authors: | , , , |
| Format: | Article |
| Language: | English |
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| container_end_page | m828 |
| container_issue | 6 |
| container_start_page | m827 |
| container_title | Acta crystallographica. Section E, Structure reports online |
| container_volume | 68 |
| creator | Bouchameni, Chahra Beghidja, Chahrazed Beghidja, Adel Boutebdja, Mehdi |
| description | The title compound, [Na(C
10
H
9.5
N
2
O
2
S
2
)
2
(H
2
O)], is a molecular sodium complex with
N
′-(1,3-dithiolan-2-yl)-2-hydroxybenzohydrazide ligands with the negative charge spread evenly over both, and a water molecule. The Na
I
ion coordination is distorted trigonal–bipyramidal, formed by two N and three O atoms, with the Na
I
ion lying on a twofold rotation axis. Intramolecular N—H...O hydrogen bonds occur. Molecules pack as discrete units and the crystal packing is stabilized by strong O—H...O hydrogen bonds, which give rise to chains along [010]; the chains are interlinked by strong O—H...O hydrogen bonds. |
| doi_str_mv | 10.1107/S1600536812023239 |
| format | article |
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10
H
9.5
N
2
O
2
S
2
)
2
(H
2
O)], is a molecular sodium complex with
N
′-(1,3-dithiolan-2-yl)-2-hydroxybenzohydrazide ligands with the negative charge spread evenly over both, and a water molecule. The Na
I
ion coordination is distorted trigonal–bipyramidal, formed by two N and three O atoms, with the Na
I
ion lying on a twofold rotation axis. Intramolecular N—H...O hydrogen bonds occur. Molecules pack as discrete units and the crystal packing is stabilized by strong O—H...O hydrogen bonds, which give rise to chains along [010]; the chains are interlinked by strong O—H...O hydrogen bonds.</description><identifier>ISSN: 1600-5368</identifier><identifier>EISSN: 1600-5368</identifier><identifier>DOI: 10.1107/S1600536812023239</identifier><language>eng</language><publisher>International Union of Crystallography</publisher><ispartof>Acta crystallographica. Section E, Structure reports online, 2012-06, Vol.68 (6), p.m827-m828</ispartof><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Bouchameni, Chahra</creatorcontrib><creatorcontrib>Beghidja, Chahrazed</creatorcontrib><creatorcontrib>Beghidja, Adel</creatorcontrib><creatorcontrib>Boutebdja, Mehdi</creatorcontrib><title>Aquabis[ N ′-(1,3-dithiolan-2-ylidene)-2-hydroxybenzohydrazidato(0.5−)-κ 2 N ′, O ]sodium(I)</title><title>Acta crystallographica. Section E, Structure reports online</title><description>The title compound, [Na(C
10
H
9.5
N
2
O
2
S
2
)
2
(H
2
O)], is a molecular sodium complex with
N
′-(1,3-dithiolan-2-yl)-2-hydroxybenzohydrazide ligands with the negative charge spread evenly over both, and a water molecule. The Na
I
ion coordination is distorted trigonal–bipyramidal, formed by two N and three O atoms, with the Na
I
ion lying on a twofold rotation axis. Intramolecular N—H...O hydrogen bonds occur. Molecules pack as discrete units and the crystal packing is stabilized by strong O—H...O hydrogen bonds, which give rise to chains along [010]; the chains are interlinked by strong O—H...O hydrogen bonds.</description><issn>1600-5368</issn><issn>1600-5368</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><sourceid>DOA</sourceid><recordid>eNplkM1Kw0AURoMoWKsP4C7LFpx678wkkyxL8adQ7EJdiYQ7mcROSTuatGC6cunaR3HpQ_gQfRIbKyK4uodz4Sw-zztG6CGCOr3GECAQYYQcuOAi3vFajWKN2_3D-95BVU0BMFQcW17af1qSttWdf-WvX95ZB08EM3Yxsa6gOeOsLqzJ5ll3g5PalO651tl85RqmlTW0cB3oBevXty77_PD5NnPij_37yhm7nHWG3UNvL6eiyo5-btu7PT-7GVyy0fhiOOiPWCogXDCFkeHSgNIi1yEKEpRLrgPMec4NpygVSm_eQJIbCABEikRGK5RcYgSi7Q23XeNomjyWdkZlnTiyybdw5UNC5cKmRZbkGMeCIIgoQClRa1JSaUQTpwQyE5sWbltp6aqqzPLfHkLSLJ78W1x8AcZCcr4</recordid><startdate>20120601</startdate><enddate>20120601</enddate><creator>Bouchameni, Chahra</creator><creator>Beghidja, Chahrazed</creator><creator>Beghidja, Adel</creator><creator>Boutebdja, Mehdi</creator><general>International Union of Crystallography</general><scope>AAYXX</scope><scope>CITATION</scope><scope>DOA</scope></search><sort><creationdate>20120601</creationdate><title>Aquabis[ N ′-(1,3-dithiolan-2-ylidene)-2-hydroxybenzohydrazidato(0.5−)-κ 2 N ′, O ]sodium(I)</title><author>Bouchameni, Chahra ; Beghidja, Chahrazed ; Beghidja, Adel ; Boutebdja, Mehdi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c306t-718d24d07b3fb613a3af42b51f2f2d2a8c37bd070a42d05003c1aadb714241803</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bouchameni, Chahra</creatorcontrib><creatorcontrib>Beghidja, Chahrazed</creatorcontrib><creatorcontrib>Beghidja, Adel</creatorcontrib><creatorcontrib>Boutebdja, Mehdi</creatorcontrib><collection>CrossRef</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>Acta crystallographica. Section E, Structure reports online</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bouchameni, Chahra</au><au>Beghidja, Chahrazed</au><au>Beghidja, Adel</au><au>Boutebdja, Mehdi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Aquabis[ N ′-(1,3-dithiolan-2-ylidene)-2-hydroxybenzohydrazidato(0.5−)-κ 2 N ′, O ]sodium(I)</atitle><jtitle>Acta crystallographica. Section E, Structure reports online</jtitle><date>2012-06-01</date><risdate>2012</risdate><volume>68</volume><issue>6</issue><spage>m827</spage><epage>m828</epage><pages>m827-m828</pages><issn>1600-5368</issn><eissn>1600-5368</eissn><abstract>The title compound, [Na(C
10
H
9.5
N
2
O
2
S
2
)
2
(H
2
O)], is a molecular sodium complex with
N
′-(1,3-dithiolan-2-yl)-2-hydroxybenzohydrazide ligands with the negative charge spread evenly over both, and a water molecule. The Na
I
ion coordination is distorted trigonal–bipyramidal, formed by two N and three O atoms, with the Na
I
ion lying on a twofold rotation axis. Intramolecular N—H...O hydrogen bonds occur. Molecules pack as discrete units and the crystal packing is stabilized by strong O—H...O hydrogen bonds, which give rise to chains along [010]; the chains are interlinked by strong O—H...O hydrogen bonds.</abstract><pub>International Union of Crystallography</pub><doi>10.1107/S1600536812023239</doi><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1600-5368 |
| ispartof | Acta crystallographica. Section E, Structure reports online, 2012-06, Vol.68 (6), p.m827-m828 |
| issn | 1600-5368 1600-5368 |
| language | eng |
| recordid | cdi_doaj_primary_oai_doaj_org_article_f1993a058a51441bba747b11d9ca04e3 |
| source | PubMed Central |
| title | Aquabis[ N ′-(1,3-dithiolan-2-ylidene)-2-hydroxybenzohydrazidato(0.5−)-κ 2 N ′, O ]sodium(I) |
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