Synthesis of N-Benzylideneaniline by Schiff base reaction using Kinnow peel powder as Green catalyst and comparative study of derivatives through ANOVA techniques

The cheap and easy availability of the Kinnow peel waste has reported various applications due to presence of multifunctional groups. Therefore, in present study we explored its application to synthesize N-Benzylideneaniline and its derivatives based on Schiff base reaction. Kinnow peel powder is ch...

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Bibliographic Details
Published in:Scientific reports 2022-06, Vol.12 (1), p.9636-9636, Article 9636
Main Authors: Verma, Renu, Lamba, Narendra Pal, Dandia, Anshu, Srivastava, Anamika, Modi, Kanak, Chauhan, Manmohan Singh, Prasad, Jagdish
Format: Article
Language:English
Subjects:
639/638
639/705
Aniline
Aniline Compounds
Benzaldehyde
Benzaldehydes
Biomass
Carbon
Catalysis
Catalysts
Chemicals
Chemistry
Comparative studies
Fourier transforms
Humanities and Social Sciences
Ligands
multidisciplinary
Nanocomposites
Nanoparticles
Powders
Scanning electron microscopy
Schiff Bases
Science
Science (multidisciplinary)
Solvents
Thermal stability
Variance analysis
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Summary:The cheap and easy availability of the Kinnow peel waste has reported various applications due to presence of multifunctional groups. Therefore, in present study we explored its application to synthesize N-Benzylideneaniline and its derivatives based on Schiff base reaction. Kinnow peel powder is characterized by FTIR, TEM, SEM, XRD, EDX, and TGA for functional groups, morphology, surface, elements and thermal stability. Benzaldehyde, aniline, and their derivatives such as 4-methyl benzaldehyde, 4-hydroxy benzaldehyde, 4-methoxy benzaldehyde, and 4-methoxy aniline have been used to compare the efficacy of the Schiff base reaction using analysis of variance (ANOVA) and it has been observed that combination of Aniline and benzaldehyde for Schiff base reaction provided 85% yield of relative product.
ISSN:2045-2322
2045-2322
DOI:10.1038/s41598-022-13360-5