Justification of the criteria requirements for fillers in mixtures for 3D construction printing

• Published in: Nanotehnologii v stroitelʹstve 2023-01, Vol.15 (4), p.310-318
• Main Authors: Slavcheva, G.S., Razov, I.O., Solonina, V.A., Panchenko, Y.F.
• Format: Article
• Language: English
• Subjects: Additive manufacturing; additive technologies; Cement; cement composites; Composite materials; Criteria; Electron microscopy; Fillers; Granular materials; Granular media; Mixtures; modelling; Particle shape; Particle size; Raw materials; Rheological properties; Rheology; Three dimensional printing
• ISSN: 2075-8545; 2075-8545
• DOI: 10.15828/2075-8545-2023-15-4-310-318

Introduction. As part of the task to create new materials for additive technologies, an analysis of the situation was carried out, and a problem was identified with the lack of common approaches to selecting raw material components for mixtures. Theoretical concept. Based on the approaches of fundamental structure rheology, physicochemical mechanics of disperse systems, the theory of packing of granular media, we theoretically justified the criteria requirements for the characteristics of fillers and suggested quantitative criteria for their evaluation. It was proposed to use these quantitative criteria for a preliminary comprehensive assessment of fillers when designing compositions of mixtures for 3D construction printing. Materials and methods. The characteristics of the fillers were evaluated using scanning electron microscopy with a scanning electron microscope Thermo Scientific™ Phenom™ Desktop SEM and processing of images by the ParticleMetric software package as well as using laser granulometry with a laser analyser of particles Analysette 22. Results. We assessed the cement and 5 types of fillers that had different sizes and played different roles in the formation of the mixture properties. We also identified their estimated criterial characteristics, including the average particle diameter, gra-nulometric constant, and particle shape coefficient. Boundary values of these characteristics were determined for particles of different morphology and dispersion degree. Conclusion. Based on the application of the suggested theoretical approaches, we determined the lines of research associated with obtaining experimental patterns of the impact of the criterial characteristics of fillers on the rheological characteristics of mixtures as well as with these characteristics according to their significance and justifying the requirements for the range of quantities of fillers depending on their size, shape, and granulometry. cement composites, additive technologies, modelling, fillers, rheology.