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Analysis of biodiesel by high performance liquid chromatography using refractive index detector
[Display omitted] High-performance liquid chromatography (HPLC) was used for the determination of compounds occurring during the production of biodiesel from karanja and jatropha oil. Methanol was used for fast monitoring of conversion of karanja and jatropha oil triacylglycerols to fatty acid methy...
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Published in: | MethodsX 2017-01, Vol.4 (C), p.256-259 |
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High-performance liquid chromatography (HPLC) was used for the determination of compounds occurring during the production of biodiesel from karanja and jatropha oil. Methanol was used for fast monitoring of conversion of karanja and jatropha oil triacylglycerols to fatty acid methyl esters and for quantitation of residual triacylglycerols (TGs), in the final biodiesel product. The individual sample compounds were identified using HPLC. Analysis of fatty acid methyl esters (FAMES) in blends of biodiesel by HPLC using a refractive index and a UV detector at 238nm. Individual triacylglycerols, diacylglycerols, monoacylglycerols and methyl esters of oleic, linoleic and linolenic acids and free fatty acids were separated within 40min. Hence HPLC was found to be best for the analysis of biodiesel. Analysis of biodiesel by HPLC using RID detector. Estimation of amount of FAMES in biodiesel. Individual triacylglycerols, diacylglycerols, monoacylglycerols and methyl esters of oleic, linoleic and linolenic acids and free fatty acids were separated within 40min. |
doi_str_mv | 10.1016/j.mex.2017.07.002 |
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High-performance liquid chromatography (HPLC) was used for the determination of compounds occurring during the production of biodiesel from karanja and jatropha oil. Methanol was used for fast monitoring of conversion of karanja and jatropha oil triacylglycerols to fatty acid methyl esters and for quantitation of residual triacylglycerols (TGs), in the final biodiesel product. The individual sample compounds were identified using HPLC. Analysis of fatty acid methyl esters (FAMES) in blends of biodiesel by HPLC using a refractive index and a UV detector at 238nm. Individual triacylglycerols, diacylglycerols, monoacylglycerols and methyl esters of oleic, linoleic and linolenic acids and free fatty acids were separated within 40min. Hence HPLC was found to be best for the analysis of biodiesel. Analysis of biodiesel by HPLC using RID detector. Estimation of amount of FAMES in biodiesel. Individual triacylglycerols, diacylglycerols, monoacylglycerols and methyl esters of oleic, linoleic and linolenic acids and free fatty acids were separated within 40min.</description><identifier>ISSN: 2215-0161</identifier><identifier>EISSN: 2215-0161</identifier><identifier>DOI: 10.1016/j.mex.2017.07.002</identifier><identifier>PMID: 28794997</identifier><language>eng</language><publisher>Netherlands: Elsevier B.V</publisher><subject>Biodiesel ; HPLC ; Method ; Refractive index ; UV detector</subject><ispartof>MethodsX, 2017-01, Vol.4 (C), p.256-259</ispartof><rights>2017</rights><rights>2017 Published by Elsevier B.V. 2017</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c517t-1867d5a8a14c072d4ead079ef17e66d2a9beebbd01fbdab076592010e331604c3</citedby><cites>FETCH-LOGICAL-c517t-1867d5a8a14c072d4ead079ef17e66d2a9beebbd01fbdab076592010e331604c3</cites><orcidid>0000-0002-3648-1497</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC5547239/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S2215016117300225$$EHTML$$P50$$Gelsevier$$Hfree_for_read</linktohtml><link.rule.ids>230,314,727,780,784,885,3549,27924,27925,45780,53791,53793</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/28794997$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Syed, Mahin Basha</creatorcontrib><title>Analysis of biodiesel by high performance liquid chromatography using refractive index detector</title><title>MethodsX</title><addtitle>MethodsX</addtitle><description>[Display omitted]
High-performance liquid chromatography (HPLC) was used for the determination of compounds occurring during the production of biodiesel from karanja and jatropha oil. Methanol was used for fast monitoring of conversion of karanja and jatropha oil triacylglycerols to fatty acid methyl esters and for quantitation of residual triacylglycerols (TGs), in the final biodiesel product. The individual sample compounds were identified using HPLC. Analysis of fatty acid methyl esters (FAMES) in blends of biodiesel by HPLC using a refractive index and a UV detector at 238nm. Individual triacylglycerols, diacylglycerols, monoacylglycerols and methyl esters of oleic, linoleic and linolenic acids and free fatty acids were separated within 40min. Hence HPLC was found to be best for the analysis of biodiesel. Analysis of biodiesel by HPLC using RID detector. Estimation of amount of FAMES in biodiesel. Individual triacylglycerols, diacylglycerols, monoacylglycerols and methyl esters of oleic, linoleic and linolenic acids and free fatty acids were separated within 40min.</description><subject>Biodiesel</subject><subject>HPLC</subject><subject>Method</subject><subject>Refractive index</subject><subject>UV detector</subject><issn>2215-0161</issn><issn>2215-0161</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><sourceid>DOA</sourceid><recordid>eNp9kU1r3DAQhk1pSUKaH5BL0bGX3czIH7IpFEJomkCgl_YsZGlka7GtjWQv2X9fbTYNyaUwoEHzzjPSvFl2ibBGwOpqsx7pac0BxRpSAP-QnXGO5SoV8eOb_DS7iHEDAJgXORb8JDvltWiKphFnmbye1LCPLjJvWeu8cRRpYO2e9a7r2ZaC9WFUkyY2uMfFGab74Ec1-y6obb9nS3RTxwLZoPTsdsTcZOiJGZpJzz58zj5ZNUS6eDnPsz-3P37f3K0efv28v7l-WOkSxbzCuhKmVLXCQoPgpiBlQDRkUVBVGa6alqhtDaBtjWpBVGWTvg6U51hBofPz7P7INV5t5Da4UYW99MrJ5wsfOqnC7PRA0qqaqKyQDFJhla3R1HBIyxpEbimxvh9Z26UdyWia5qCGd9D3lcn1svM7WZaF4HmTAF9fAME_LhRnObqoaRjURH6JEhsu6lwUmCcpHqU6-BjTGl_HIMiDz3Ijk8_y4LOEFMBTz5e373vt-OdqEnw7CihtfOcoyKgdJQ-NC8mVtBL3H_xfl8-7nw</recordid><startdate>20170101</startdate><enddate>20170101</enddate><creator>Syed, Mahin Basha</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>6I.</scope><scope>AAFTH</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>5PM</scope><scope>DOA</scope><orcidid>https://orcid.org/0000-0002-3648-1497</orcidid></search><sort><creationdate>20170101</creationdate><title>Analysis of biodiesel by high performance liquid chromatography using refractive index detector</title><author>Syed, Mahin Basha</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c517t-1867d5a8a14c072d4ead079ef17e66d2a9beebbd01fbdab076592010e331604c3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Biodiesel</topic><topic>HPLC</topic><topic>Method</topic><topic>Refractive index</topic><topic>UV detector</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Syed, Mahin Basha</creatorcontrib><collection>ScienceDirect Open Access Titles</collection><collection>Elsevier:ScienceDirect:Open Access</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>MethodsX</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Syed, Mahin Basha</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Analysis of biodiesel by high performance liquid chromatography using refractive index detector</atitle><jtitle>MethodsX</jtitle><addtitle>MethodsX</addtitle><date>2017-01-01</date><risdate>2017</risdate><volume>4</volume><issue>C</issue><spage>256</spage><epage>259</epage><pages>256-259</pages><issn>2215-0161</issn><eissn>2215-0161</eissn><abstract>[Display omitted]
High-performance liquid chromatography (HPLC) was used for the determination of compounds occurring during the production of biodiesel from karanja and jatropha oil. Methanol was used for fast monitoring of conversion of karanja and jatropha oil triacylglycerols to fatty acid methyl esters and for quantitation of residual triacylglycerols (TGs), in the final biodiesel product. The individual sample compounds were identified using HPLC. Analysis of fatty acid methyl esters (FAMES) in blends of biodiesel by HPLC using a refractive index and a UV detector at 238nm. Individual triacylglycerols, diacylglycerols, monoacylglycerols and methyl esters of oleic, linoleic and linolenic acids and free fatty acids were separated within 40min. Hence HPLC was found to be best for the analysis of biodiesel. Analysis of biodiesel by HPLC using RID detector. Estimation of amount of FAMES in biodiesel. Individual triacylglycerols, diacylglycerols, monoacylglycerols and methyl esters of oleic, linoleic and linolenic acids and free fatty acids were separated within 40min.</abstract><cop>Netherlands</cop><pub>Elsevier B.V</pub><pmid>28794997</pmid><doi>10.1016/j.mex.2017.07.002</doi><tpages>4</tpages><orcidid>https://orcid.org/0000-0002-3648-1497</orcidid><oa>free_for_read</oa></addata></record> |
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subjects | Biodiesel HPLC Method Refractive index UV detector |
title | Analysis of biodiesel by high performance liquid chromatography using refractive index detector |
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