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Synthesis and Properties of Selected Energetic Organodi- and Polyammonium Nitrate Salts
The objective of this program was to synthesize and characterize selected organodi- and polyammonium nitrate salts for use in a qualitative study of thermal and impact stability characteristics. A total of twenty-two salts were prepared and characterized. A literature search confirmed that fifteen o...
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| creator | Hildreth, Robert A Fryling, James A Struck, Stephen R McKenney, Robert L , Jr |
| description | The objective of this program was to synthesize and characterize selected organodi- and polyammonium nitrate salts for use in a qualitative study of thermal and impact stability characteristics. A total of twenty-two salts were prepared and characterized. A literature search confirmed that fifteen of these materials had never been reported and, therefore, were assumed to be original. The general synthetic process is described with specific details for each compound included. Elemental analyses are provided for the new compounds as well as their nuclear magnetic resonance spectra. Other data included are densities (calculated and measured), heats of fusion, melting points, and the temperature of the major peak associated with exothermic decomposition as measured by a differential scanning calorimeter. |
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A total of twenty-two salts were prepared and characterized. A literature search confirmed that fifteen of these materials had never been reported and, therefore, were assumed to be original. The general synthetic process is described with specific details for each compound included. Elemental analyses are provided for the new compounds as well as their nuclear magnetic resonance spectra. Other data included are densities (calculated and measured), heats of fusion, melting points, and the temperature of the major peak associated with exothermic decomposition as measured by a differential scanning calorimeter.</description><language>eng</language><subject>AMMONIUM NITRATE ; Ammunition and Explosives ; DENSITY ; DIAMMONIUM NITRATE SALTS ; ENERGETIC NITRATE SALTS ; EQUATIONS ; EXOTHERMIC DECOMPOSITION ; EXPLOSIVES ; FY86 ; HEAT OF FUSION ; IMPACT STABILITY ; Industrial Chemistry and Chemical Processing ; Inorganic Chemistry ; INORGANIC COMPOUNDS ; LITERATURE SURVEYS ; MELTING POINT ; NMR(NUCLEAR MAGNETIC RESONANCE) ; Organic Chemistry ; ORGANIC COMPOUNDS ; PE62602F ; POLYAMMONIUM NITRATE SALTS ; QUALITATIVE ANALYSIS ; SENSITIVITY ; SYNTHESIS(CHEMISTRY) ; TEMPERATURE ; THERMAL STABILITY ; WUAFATL25021012</subject><creationdate>1986</creationdate><rights>APPROVED FOR PUBLIC RELEASE</rights><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,780,885,27567,27568</link.rule.ids><linktorsrc>$$Uhttps://apps.dtic.mil/sti/citations/ADA167224$$EView_record_in_DTIC$$FView_record_in_$$GDTIC$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>Hildreth, Robert A</creatorcontrib><creatorcontrib>Fryling, James A</creatorcontrib><creatorcontrib>Struck, Stephen R</creatorcontrib><creatorcontrib>McKenney, Robert L , Jr</creatorcontrib><creatorcontrib>AIR FORCE ARMAMENT LAB EGLIN AFB FL ENERGETIC MATERIALS BRANCH</creatorcontrib><title>Synthesis and Properties of Selected Energetic Organodi- and Polyammonium Nitrate Salts</title><description>The objective of this program was to synthesize and characterize selected organodi- and polyammonium nitrate salts for use in a qualitative study of thermal and impact stability characteristics. A total of twenty-two salts were prepared and characterized. A literature search confirmed that fifteen of these materials had never been reported and, therefore, were assumed to be original. The general synthetic process is described with specific details for each compound included. Elemental analyses are provided for the new compounds as well as their nuclear magnetic resonance spectra. Other data included are densities (calculated and measured), heats of fusion, melting points, and the temperature of the major peak associated with exothermic decomposition as measured by a differential scanning calorimeter.</description><subject>AMMONIUM NITRATE</subject><subject>Ammunition and Explosives</subject><subject>DENSITY</subject><subject>DIAMMONIUM NITRATE SALTS</subject><subject>ENERGETIC NITRATE SALTS</subject><subject>EQUATIONS</subject><subject>EXOTHERMIC DECOMPOSITION</subject><subject>EXPLOSIVES</subject><subject>FY86</subject><subject>HEAT OF FUSION</subject><subject>IMPACT STABILITY</subject><subject>Industrial Chemistry and Chemical Processing</subject><subject>Inorganic Chemistry</subject><subject>INORGANIC COMPOUNDS</subject><subject>LITERATURE SURVEYS</subject><subject>MELTING POINT</subject><subject>NMR(NUCLEAR MAGNETIC RESONANCE)</subject><subject>Organic Chemistry</subject><subject>ORGANIC COMPOUNDS</subject><subject>PE62602F</subject><subject>POLYAMMONIUM NITRATE SALTS</subject><subject>QUALITATIVE ANALYSIS</subject><subject>SENSITIVITY</subject><subject>SYNTHESIS(CHEMISTRY)</subject><subject>TEMPERATURE</subject><subject>THERMAL STABILITY</subject><subject>WUAFATL25021012</subject><fulltext>true</fulltext><rsrctype>report</rsrctype><creationdate>1986</creationdate><recordtype>report</recordtype><sourceid>1RU</sourceid><recordid>eNqFjDEKwkAQANNYiPoDi_1ACqNoHTRipcIJlmHJbeLC3Z7crkV-r6C91RQzzLS4u1HsQcoKKB6uOT0pG5NC6sFRoM7IQyOUBzLu4JIHlOS5_OYpjBhjEn5FOLNlNAKHwXReTHoMSosfZ8Xy2Nz2p9J_Lq0aC1lbH-rVdldVm_Uf_QYKIjbc</recordid><startdate>198604</startdate><enddate>198604</enddate><creator>Hildreth, Robert A</creator><creator>Fryling, James A</creator><creator>Struck, Stephen R</creator><creator>McKenney, Robert L , Jr</creator><scope>1RU</scope><scope>BHM</scope></search><sort><creationdate>198604</creationdate><title>Synthesis and Properties of Selected Energetic Organodi- and Polyammonium Nitrate Salts</title><author>Hildreth, Robert A ; Fryling, James A ; Struck, Stephen R ; McKenney, Robert L , Jr</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-dtic_stinet_ADA1672243</frbrgroupid><rsrctype>reports</rsrctype><prefilter>reports</prefilter><language>eng</language><creationdate>1986</creationdate><topic>AMMONIUM NITRATE</topic><topic>Ammunition and Explosives</topic><topic>DENSITY</topic><topic>DIAMMONIUM NITRATE SALTS</topic><topic>ENERGETIC NITRATE SALTS</topic><topic>EQUATIONS</topic><topic>EXOTHERMIC DECOMPOSITION</topic><topic>EXPLOSIVES</topic><topic>FY86</topic><topic>HEAT OF FUSION</topic><topic>IMPACT STABILITY</topic><topic>Industrial Chemistry and Chemical Processing</topic><topic>Inorganic Chemistry</topic><topic>INORGANIC COMPOUNDS</topic><topic>LITERATURE SURVEYS</topic><topic>MELTING POINT</topic><topic>NMR(NUCLEAR MAGNETIC RESONANCE)</topic><topic>Organic Chemistry</topic><topic>ORGANIC COMPOUNDS</topic><topic>PE62602F</topic><topic>POLYAMMONIUM NITRATE SALTS</topic><topic>QUALITATIVE ANALYSIS</topic><topic>SENSITIVITY</topic><topic>SYNTHESIS(CHEMISTRY)</topic><topic>TEMPERATURE</topic><topic>THERMAL STABILITY</topic><topic>WUAFATL25021012</topic><toplevel>online_resources</toplevel><creatorcontrib>Hildreth, Robert A</creatorcontrib><creatorcontrib>Fryling, James A</creatorcontrib><creatorcontrib>Struck, Stephen R</creatorcontrib><creatorcontrib>McKenney, Robert L , Jr</creatorcontrib><creatorcontrib>AIR FORCE ARMAMENT LAB EGLIN AFB FL ENERGETIC MATERIALS BRANCH</creatorcontrib><collection>DTIC Technical Reports</collection><collection>DTIC STINET</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>Hildreth, Robert A</au><au>Fryling, James A</au><au>Struck, Stephen R</au><au>McKenney, Robert L , Jr</au><aucorp>AIR FORCE ARMAMENT LAB EGLIN AFB FL ENERGETIC MATERIALS BRANCH</aucorp><format>book</format><genre>unknown</genre><ristype>RPRT</ristype><btitle>Synthesis and Properties of Selected Energetic Organodi- and Polyammonium Nitrate Salts</btitle><date>1986-04</date><risdate>1986</risdate><abstract>The objective of this program was to synthesize and characterize selected organodi- and polyammonium nitrate salts for use in a qualitative study of thermal and impact stability characteristics. A total of twenty-two salts were prepared and characterized. A literature search confirmed that fifteen of these materials had never been reported and, therefore, were assumed to be original. The general synthetic process is described with specific details for each compound included. Elemental analyses are provided for the new compounds as well as their nuclear magnetic resonance spectra. Other data included are densities (calculated and measured), heats of fusion, melting points, and the temperature of the major peak associated with exothermic decomposition as measured by a differential scanning calorimeter.</abstract><oa>free_for_read</oa></addata></record> |
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| source | DTIC Technical Reports |
| subjects | AMMONIUM NITRATE Ammunition and Explosives DENSITY DIAMMONIUM NITRATE SALTS ENERGETIC NITRATE SALTS EQUATIONS EXOTHERMIC DECOMPOSITION EXPLOSIVES FY86 HEAT OF FUSION IMPACT STABILITY Industrial Chemistry and Chemical Processing Inorganic Chemistry INORGANIC COMPOUNDS LITERATURE SURVEYS MELTING POINT NMR(NUCLEAR MAGNETIC RESONANCE) Organic Chemistry ORGANIC COMPOUNDS PE62602F POLYAMMONIUM NITRATE SALTS QUALITATIVE ANALYSIS SENSITIVITY SYNTHESIS(CHEMISTRY) TEMPERATURE THERMAL STABILITY WUAFATL25021012 |
| title | Synthesis and Properties of Selected Energetic Organodi- and Polyammonium Nitrate Salts |
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