Single Lithium Ion Conducting Polymer Electrolyte

Because of the importance of this starting material, considerable effort was expended on modification of the reported workup. Elimination of all extraction and careful acidification of the diluted reaction mixture at low temperature leads to a consistent 40-50% yield of product exhibiting the charac...

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Bibliographic Details
Main Authors: Feld, William A, Weimers, Denise M
Format: Report
Language:English
Subjects:
ANTHRACENES
ANTHRACYLINES
ANTIBIOTICS
COMPUTATIONAL CHEMISTRY
Electrochemical Energy Storage
LITHIUM BATTERIES
MODIFICATION
NAPHTHALENES
Organic Chemistry
PE61102F
Physical Chemistry
POLYELECTROLYTES
POLYMER ELECTROLYTES
PORPHYRINS
SYNTHESIS(CHEMISTRY)
WUAFOSR2303BV
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Description
Summary:Because of the importance of this starting material, considerable effort was expended on modification of the reported workup. Elimination of all extraction and careful acidification of the diluted reaction mixture at low temperature leads to a consistent 40-50% yield of product exhibiting the characteristics of previously prepared samples. In addition to our interest in this material it appears to be an important starting material for the synthesis of anthracycline intermediates. Anthracyclines are used as antitumor antibiotics (c.f., Henry, D.W., Cancer. Treat. Rep 1979, 63, 845) in which they act as DNA intercalators. A publication specifying the details of the synthesis and workup is being prepared.