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Thermal studies on solid 1,4-bis(3-carboxy-3-oxo-prop-1-enyl) benzene of lighter trivalent lanthanides
Solid-state compounds of general formula Ln 2 L 3 · n H 2 O, where L represents 1,4-bis(3-carboxy-3-oxo-prop-1-enyl)benzene and Ln = La, Ce, Pr, Nd, Sm, were synthesized. Complexometric titrations with EDTA, thermogravimetry (TG), differential thermal analysis (DTA), differential scanning calorimetr...
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| Published in: | Journal of thermal analysis and calorimetry 2011-11, Vol.106 (2), p.525-529 |
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| Main Authors: | , , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c391t-7eb1dfbbfa0a18b84c947a2a672a10782de30944607224cdd093adc0e7be90c3 |
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| cites | cdi_FETCH-LOGICAL-c391t-7eb1dfbbfa0a18b84c947a2a672a10782de30944607224cdd093adc0e7be90c3 |
| container_end_page | 529 |
| container_issue | 2 |
| container_start_page | 525 |
| container_title | Journal of thermal analysis and calorimetry |
| container_volume | 106 |
| creator | Nunes, Ronaldo S. Bannach, Gilbert Luiz, José M. Caires, Flávio J. Carvalho, Claudio T. Ionashiro, Massao |
| description | Solid-state compounds of general formula Ln
2
L
3
·
n
H
2
O, where L represents 1,4-bis(3-carboxy-3-oxo-prop-1-enyl)benzene and Ln = La, Ce, Pr, Nd, Sm, were synthesized. Complexometric titrations with EDTA, thermogravimetry (TG), differential thermal analysis (DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, elemental analysis and infrared spectroscopy have been employed to characterize and to study the thermal behavior of these compounds in dynamic air atmosphere. The results led to information about the composition, dehydration, crystallinity, and thermal decomposition of the synthesized compounds. |
| doi_str_mv | 10.1007/s10973-010-1250-6 |
| format | article |
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2
L
3
·
n
H
2
O, where L represents 1,4-bis(3-carboxy-3-oxo-prop-1-enyl)benzene and Ln = La, Ce, Pr, Nd, Sm, were synthesized. Complexometric titrations with EDTA, thermogravimetry (TG), differential thermal analysis (DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, elemental analysis and infrared spectroscopy have been employed to characterize and to study the thermal behavior of these compounds in dynamic air atmosphere. The results led to information about the composition, dehydration, crystallinity, and thermal decomposition of the synthesized compounds.</description><identifier>ISSN: 1388-6150</identifier><identifier>EISSN: 1588-2926</identifier><identifier>EISSN: 1572-8943</identifier><identifier>DOI: 10.1007/s10973-010-1250-6</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Analysis ; Analytical Chemistry ; Benzene ; Chemical properties ; Chemistry ; Chemistry and Materials Science ; Coordination compounds ; Exact sciences and technology ; Inorganic Chemistry ; Inorganic chemistry and origins of life ; Measurement Science and Instrumentation ; Physical Chemistry ; Polymer Sciences ; Preparations and properties ; Thermodynamics</subject><ispartof>Journal of thermal analysis and calorimetry, 2011-11, Vol.106 (2), p.525-529</ispartof><rights>Akadémiai Kiadó, Budapest, Hungary 2011</rights><rights>2015 INIST-CNRS</rights><rights>COPYRIGHT 2011 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c391t-7eb1dfbbfa0a18b84c947a2a672a10782de30944607224cdd093adc0e7be90c3</citedby><cites>FETCH-LOGICAL-c391t-7eb1dfbbfa0a18b84c947a2a672a10782de30944607224cdd093adc0e7be90c3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>309,310,314,780,784,789,790,23930,23931,25140,27924,27925</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=24740369$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Nunes, Ronaldo S.</creatorcontrib><creatorcontrib>Bannach, Gilbert</creatorcontrib><creatorcontrib>Luiz, José M.</creatorcontrib><creatorcontrib>Caires, Flávio J.</creatorcontrib><creatorcontrib>Carvalho, Claudio T.</creatorcontrib><creatorcontrib>Ionashiro, Massao</creatorcontrib><title>Thermal studies on solid 1,4-bis(3-carboxy-3-oxo-prop-1-enyl) benzene of lighter trivalent lanthanides</title><title>Journal of thermal analysis and calorimetry</title><addtitle>J Therm Anal Calorim</addtitle><description>Solid-state compounds of general formula Ln
2
L
3
·
n
H
2
O, where L represents 1,4-bis(3-carboxy-3-oxo-prop-1-enyl)benzene and Ln = La, Ce, Pr, Nd, Sm, were synthesized. Complexometric titrations with EDTA, thermogravimetry (TG), differential thermal analysis (DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, elemental analysis and infrared spectroscopy have been employed to characterize and to study the thermal behavior of these compounds in dynamic air atmosphere. The results led to information about the composition, dehydration, crystallinity, and thermal decomposition of the synthesized compounds.</description><subject>Analysis</subject><subject>Analytical Chemistry</subject><subject>Benzene</subject><subject>Chemical properties</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Coordination compounds</subject><subject>Exact sciences and technology</subject><subject>Inorganic Chemistry</subject><subject>Inorganic chemistry and origins of life</subject><subject>Measurement Science and Instrumentation</subject><subject>Physical Chemistry</subject><subject>Polymer Sciences</subject><subject>Preparations and properties</subject><subject>Thermodynamics</subject><issn>1388-6150</issn><issn>1588-2926</issn><issn>1572-8943</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNp9kV1rHCEUhofSQkOSH9A7bwoN1PSoM-N4GUI_AoFCu_fix3HXMquLzpbd_voaphRyE7zwqM9zUN-ue8fglgHIT5WBkoICA8r4AHR81V2wYZooV3x83WrR6pEN8La7rjVa4AxGNUzqogubHZa9mUldjj5iJTmRmufoCfvYUxvrB0GdKTafzlTQfMr0UPKBMorpPN8Qi-kPJiQ5kDludwsWspT428yYFjKbtOxMih7rVfcmmLni9b_5stt8-by5_0Yfv399uL97pE4otlCJlvlgbTBg2GSn3qleGm5GyQ0DOXGPAlTfjyA57533oITxDlBaVODEZXe7tt22G-iYQl6KcW143EeXE4bY9u9Ee7qaBmBNuHkmNGbB07I1x1r1w88fz1m2sq7kWgsGfShxb8pZM9BPOeg1Bw1P65aDHpvzfnUOpjozh2KSi_W_yHvZgxhV4_jK1XaUtlj0r3wsqX3VC83_AnNClpw</recordid><startdate>20111101</startdate><enddate>20111101</enddate><creator>Nunes, Ronaldo S.</creator><creator>Bannach, Gilbert</creator><creator>Luiz, José M.</creator><creator>Caires, Flávio J.</creator><creator>Carvalho, Claudio T.</creator><creator>Ionashiro, Massao</creator><general>Springer Netherlands</general><general>Springer</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope></search><sort><creationdate>20111101</creationdate><title>Thermal studies on solid 1,4-bis(3-carboxy-3-oxo-prop-1-enyl) benzene of lighter trivalent lanthanides</title><author>Nunes, Ronaldo S. ; Bannach, Gilbert ; Luiz, José M. ; Caires, Flávio J. ; Carvalho, Claudio T. ; Ionashiro, Massao</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c391t-7eb1dfbbfa0a18b84c947a2a672a10782de30944607224cdd093adc0e7be90c3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Analysis</topic><topic>Analytical Chemistry</topic><topic>Benzene</topic><topic>Chemical properties</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Coordination compounds</topic><topic>Exact sciences and technology</topic><topic>Inorganic Chemistry</topic><topic>Inorganic chemistry and origins of life</topic><topic>Measurement Science and Instrumentation</topic><topic>Physical Chemistry</topic><topic>Polymer Sciences</topic><topic>Preparations and properties</topic><topic>Thermodynamics</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Nunes, Ronaldo S.</creatorcontrib><creatorcontrib>Bannach, Gilbert</creatorcontrib><creatorcontrib>Luiz, José M.</creatorcontrib><creatorcontrib>Caires, Flávio J.</creatorcontrib><creatorcontrib>Carvalho, Claudio T.</creatorcontrib><creatorcontrib>Ionashiro, Massao</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Gale In Context: Science</collection><jtitle>Journal of thermal analysis and calorimetry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Nunes, Ronaldo S.</au><au>Bannach, Gilbert</au><au>Luiz, José M.</au><au>Caires, Flávio J.</au><au>Carvalho, Claudio T.</au><au>Ionashiro, Massao</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Thermal studies on solid 1,4-bis(3-carboxy-3-oxo-prop-1-enyl) benzene of lighter trivalent lanthanides</atitle><jtitle>Journal of thermal analysis and calorimetry</jtitle><stitle>J Therm Anal Calorim</stitle><date>2011-11-01</date><risdate>2011</risdate><volume>106</volume><issue>2</issue><spage>525</spage><epage>529</epage><pages>525-529</pages><issn>1388-6150</issn><eissn>1588-2926</eissn><eissn>1572-8943</eissn><abstract>Solid-state compounds of general formula Ln
2
L
3
·
n
H
2
O, where L represents 1,4-bis(3-carboxy-3-oxo-prop-1-enyl)benzene and Ln = La, Ce, Pr, Nd, Sm, were synthesized. Complexometric titrations with EDTA, thermogravimetry (TG), differential thermal analysis (DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, elemental analysis and infrared spectroscopy have been employed to characterize and to study the thermal behavior of these compounds in dynamic air atmosphere. The results led to information about the composition, dehydration, crystallinity, and thermal decomposition of the synthesized compounds.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s10973-010-1250-6</doi><tpages>5</tpages></addata></record> |
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| identifier | ISSN: 1388-6150 |
| ispartof | Journal of thermal analysis and calorimetry, 2011-11, Vol.106 (2), p.525-529 |
| issn | 1388-6150 1588-2926 1572-8943 |
| language | eng |
| recordid | cdi_gale_infotracacademiconefile_A358998501 |
| source | Springer Nature |
| subjects | Analysis Analytical Chemistry Benzene Chemical properties Chemistry Chemistry and Materials Science Coordination compounds Exact sciences and technology Inorganic Chemistry Inorganic chemistry and origins of life Measurement Science and Instrumentation Physical Chemistry Polymer Sciences Preparations and properties Thermodynamics |
| title | Thermal studies on solid 1,4-bis(3-carboxy-3-oxo-prop-1-enyl) benzene of lighter trivalent lanthanides |
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