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Elemental composition and microstructure analysis of a rabbit urolith

Following physical examination and radiography analysis, cystotomy was performed to remove a rabbit’s single bladder stone. This rabbit urolith was analyzed by X-ray fluorescence spectrometry (EDXRF) and scanning electron microscopy (SEM). The EDXRF technique was successful for the determination of...

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Bibliographic Details
Published in:Journal of radioanalytical and nuclear chemistry 2014-10, Vol.302 (1), p.97-102
Main Authors: Machado, Débora Bellini, Sato, Ivone M., Silva, Flávia R. O., Salvador, Vera Lúcia R., Marumo, Júlio Takehiro, Schor, Nestor, Bellini, Maria Helena
Format: Article
Language:English
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Summary:Following physical examination and radiography analysis, cystotomy was performed to remove a rabbit’s single bladder stone. This rabbit urolith was analyzed by X-ray fluorescence spectrometry (EDXRF) and scanning electron microscopy (SEM). The EDXRF technique was successful for the determination of major elements (Ca, Mg, P, K and S) and presented sufficient sensitivity to also trace elements (Sr, Fe, Cu, V, Cr, Mn, Zn and Pb) determination. The results showed significant quantitative and structural variations among the urolith regions. The EDXRF technique using the fundamental parameters method and SEM attend as complementary techniques that can be useful in the management of urinary stone analysis.
ISSN:0236-5731
1588-2780
DOI:10.1007/s10967-014-3305-9