Synthetic TRP[O.sub.4] crystals as reference samples in the quantitative X-ray electron probe microanalysis of rare-earth elements

Crystals of 15 rare-earth element phosphates, which provide a set of standard reference samples in X-ray electron probe microanalysis, were synthesized and tested for homogeneity and stoichiometry. The phosphates were synthesized in two stages, the preparation of aqueous phosphates and crystal growt...

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Published in:Journal of analytical chemistry (New York, N.Y.) N.Y.), 2011-09, Vol.66 (9), p.831
Main Authors: Lavrent'ev, Yu. G, Romanenko, I.M, Novikov, M.P, Usova, L.V, Korolyuk, V.N
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Language:English
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Phosphates
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container_title Journal of analytical chemistry (New York, N.Y.)
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Romanenko, I.M
Novikov, M.P
Usova, L.V
Korolyuk, V.N
description Crystals of 15 rare-earth element phosphates, which provide a set of standard reference samples in X-ray electron probe microanalysis, were synthesized and tested for homogeneity and stoichiometry. The phosphates were synthesized in two stages, the preparation of aqueous phosphates and crystal growth in a solution of potassium polymolybdate [K.sub.2][Mo.sub.3][O.sub.10]. The tests of the synthesized crystals confirmed their reliability as reference samples.
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Phosphates
title Synthetic TRP[O.sub.4] crystals as reference samples in the quantitative X-ray electron probe microanalysis of rare-earth elements
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