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Study on electrochemical profiles of Valeriana medicinal plants by capillary electrophoresis
The objective of this work was to develop a high-performance capillary electrophoresis with amperometric detection ( CE-AD ) method for the determination of pharmacologically active ingredients in extracts of Valeriana medicinal plants. The method was validated for linearity, repeatability, limits o...
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Published in: | Journal of analytical chemistry (New York, N.Y.) N.Y.), 2014-02, Vol.69 (2), p.179-186 |
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container_end_page | 186 |
container_issue | 2 |
container_start_page | 179 |
container_title | Journal of analytical chemistry (New York, N.Y.) |
container_volume | 69 |
creator | Li, W. L. Li, M. J. Pan, Y. L. Huang, B. K. Chu, Q. C. Ye, J. N. |
description | The objective of this work was to develop a high-performance capillary electrophoresis with amperometric detection (
CE-AD
) method for the determination of pharmacologically active ingredients in extracts of
Valeriana
medicinal plants. The method was validated for linearity, repeatability, limits of detection (
LODs
) and limits of quantification (
LOQs
), etc. The LODs and LOQs of eight compounds were found to be in the range from 1.0 × 10
−8
to 1.2 × 10
−7
and 3.3 × 10
−8
to 4.0 × 10
−7
g/mL, respectively. The proposed method was successfully applied for the analyses and comparison of bioactive components in
Valeriana
samples after a relatively simple extraction procedure, and the resultant “electrochemical profiles” can intuitively demonstrate the content diversity of each electrochemically active ingredient in
Valeriana
samples from different places and plant parts. It was found the content of bioactive ingredients may vary by an order of magnitude depending on natural conditions, e.g. soil, climate, humidity etc. |
doi_str_mv | 10.1134/S1061934814020099 |
format | article |
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CE-AD
) method for the determination of pharmacologically active ingredients in extracts of
Valeriana
medicinal plants. The method was validated for linearity, repeatability, limits of detection (
LODs
) and limits of quantification (
LOQs
), etc. The LODs and LOQs of eight compounds were found to be in the range from 1.0 × 10
−8
to 1.2 × 10
−7
and 3.3 × 10
−8
to 4.0 × 10
−7
g/mL, respectively. The proposed method was successfully applied for the analyses and comparison of bioactive components in
Valeriana
samples after a relatively simple extraction procedure, and the resultant “electrochemical profiles” can intuitively demonstrate the content diversity of each electrochemically active ingredient in
Valeriana
samples from different places and plant parts. It was found the content of bioactive ingredients may vary by an order of magnitude depending on natural conditions, e.g. soil, climate, humidity etc.</description><identifier>ISSN: 1061-9348</identifier><identifier>EISSN: 1608-3199</identifier><identifier>DOI: 10.1134/S1061934814020099</identifier><language>eng</language><publisher>Boston: Springer US</publisher><subject>Analysis ; Analytical Chemistry ; Chemical properties ; Chemistry ; Chemistry and Materials Science ; Electric properties ; Medicinal plants ; Medicine, Botanic ; Medicine, Herbal ; Physiological aspects</subject><ispartof>Journal of analytical chemistry (New York, N.Y.), 2014-02, Vol.69 (2), p.179-186</ispartof><rights>Pleiades Publishing, Ltd. 2014</rights><rights>COPYRIGHT 2014 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c475t-255feba24e6798c5bd78bcb4574cd6b6e4e15d977120434552d4f1907c5c6bd23</citedby><cites>FETCH-LOGICAL-c475t-255feba24e6798c5bd78bcb4574cd6b6e4e15d977120434552d4f1907c5c6bd23</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Li, W. L.</creatorcontrib><creatorcontrib>Li, M. J.</creatorcontrib><creatorcontrib>Pan, Y. L.</creatorcontrib><creatorcontrib>Huang, B. K.</creatorcontrib><creatorcontrib>Chu, Q. C.</creatorcontrib><creatorcontrib>Ye, J. N.</creatorcontrib><title>Study on electrochemical profiles of Valeriana medicinal plants by capillary electrophoresis</title><title>Journal of analytical chemistry (New York, N.Y.)</title><addtitle>J Anal Chem</addtitle><description>The objective of this work was to develop a high-performance capillary electrophoresis with amperometric detection (
CE-AD
) method for the determination of pharmacologically active ingredients in extracts of
Valeriana
medicinal plants. The method was validated for linearity, repeatability, limits of detection (
LODs
) and limits of quantification (
LOQs
), etc. The LODs and LOQs of eight compounds were found to be in the range from 1.0 × 10
−8
to 1.2 × 10
−7
and 3.3 × 10
−8
to 4.0 × 10
−7
g/mL, respectively. The proposed method was successfully applied for the analyses and comparison of bioactive components in
Valeriana
samples after a relatively simple extraction procedure, and the resultant “electrochemical profiles” can intuitively demonstrate the content diversity of each electrochemically active ingredient in
Valeriana
samples from different places and plant parts. It was found the content of bioactive ingredients may vary by an order of magnitude depending on natural conditions, e.g. soil, climate, humidity etc.</description><subject>Analysis</subject><subject>Analytical Chemistry</subject><subject>Chemical properties</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Electric properties</subject><subject>Medicinal plants</subject><subject>Medicine, Botanic</subject><subject>Medicine, Herbal</subject><subject>Physiological aspects</subject><issn>1061-9348</issn><issn>1608-3199</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNp9kV9LwzAUxYsoOKcfwLeCTz50Jm3StI9D_DMYCE59EkKa3HYZaVOSDty3N2X6MBxyH3Lh_M7l5p4ousZohnFG7lYY5bjMSIEJShEqy5NognNUJBkuy9PQBzkZ9fPowvsNCkiB80n0uRq2ahfbLgYDcnBWrqHVUpi4d7bWBnxs6_hDGHBadCJuQWmpu1E3oht8XO1iKXptjHC73xn92jrw2l9GZ7UwHq5-3mn0_vjwdv-cLF-eFvfzZSIJo0OSUlpDJVICOSsLSSvFikpWhDIiVV7lQABTVTKGU0QyQmmqSI1LxCSVeaXSbBrd7Oc2YU-uu9oOTshWe8nnGSMYIcLyQCVHqAY6cMLYDsbfHvKzI3woNV7oqOH2wBCYAb6GRmy954vV6yGL96x01nsHNe-dbsMNOUZ8TJT_STR40r3HB7ZrwPGN3bqQhf_H9A2RFaEK</recordid><startdate>20140201</startdate><enddate>20140201</enddate><creator>Li, W. L.</creator><creator>Li, M. J.</creator><creator>Pan, Y. L.</creator><creator>Huang, B. K.</creator><creator>Chu, Q. C.</creator><creator>Ye, J. N.</creator><general>Springer US</general><general>Springer</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope></search><sort><creationdate>20140201</creationdate><title>Study on electrochemical profiles of Valeriana medicinal plants by capillary electrophoresis</title><author>Li, W. L. ; Li, M. J. ; Pan, Y. L. ; Huang, B. K. ; Chu, Q. C. ; Ye, J. N.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c475t-255feba24e6798c5bd78bcb4574cd6b6e4e15d977120434552d4f1907c5c6bd23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Analysis</topic><topic>Analytical Chemistry</topic><topic>Chemical properties</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Electric properties</topic><topic>Medicinal plants</topic><topic>Medicine, Botanic</topic><topic>Medicine, Herbal</topic><topic>Physiological aspects</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Li, W. L.</creatorcontrib><creatorcontrib>Li, M. J.</creatorcontrib><creatorcontrib>Pan, Y. L.</creatorcontrib><creatorcontrib>Huang, B. K.</creatorcontrib><creatorcontrib>Chu, Q. C.</creatorcontrib><creatorcontrib>Ye, J. N.</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><jtitle>Journal of analytical chemistry (New York, N.Y.)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Li, W. L.</au><au>Li, M. J.</au><au>Pan, Y. L.</au><au>Huang, B. K.</au><au>Chu, Q. C.</au><au>Ye, J. N.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Study on electrochemical profiles of Valeriana medicinal plants by capillary electrophoresis</atitle><jtitle>Journal of analytical chemistry (New York, N.Y.)</jtitle><stitle>J Anal Chem</stitle><date>2014-02-01</date><risdate>2014</risdate><volume>69</volume><issue>2</issue><spage>179</spage><epage>186</epage><pages>179-186</pages><issn>1061-9348</issn><eissn>1608-3199</eissn><abstract>The objective of this work was to develop a high-performance capillary electrophoresis with amperometric detection (
CE-AD
) method for the determination of pharmacologically active ingredients in extracts of
Valeriana
medicinal plants. The method was validated for linearity, repeatability, limits of detection (
LODs
) and limits of quantification (
LOQs
), etc. The LODs and LOQs of eight compounds were found to be in the range from 1.0 × 10
−8
to 1.2 × 10
−7
and 3.3 × 10
−8
to 4.0 × 10
−7
g/mL, respectively. The proposed method was successfully applied for the analyses and comparison of bioactive components in
Valeriana
samples after a relatively simple extraction procedure, and the resultant “electrochemical profiles” can intuitively demonstrate the content diversity of each electrochemically active ingredient in
Valeriana
samples from different places and plant parts. It was found the content of bioactive ingredients may vary by an order of magnitude depending on natural conditions, e.g. soil, climate, humidity etc.</abstract><cop>Boston</cop><pub>Springer US</pub><doi>10.1134/S1061934814020099</doi><tpages>8</tpages></addata></record> |
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issn | 1061-9348 1608-3199 |
language | eng |
recordid | cdi_gale_infotracmisc_A374100476 |
source | Springer Link |
subjects | Analysis Analytical Chemistry Chemical properties Chemistry Chemistry and Materials Science Electric properties Medicinal plants Medicine, Botanic Medicine, Herbal Physiological aspects |
title | Study on electrochemical profiles of Valeriana medicinal plants by capillary electrophoresis |
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