Combined Analysis of Angelica acutiloba Kitagawa Seed Oil by GC(RI), GC/MS and 13C-NMR

The seed oil of Angelica acutiloba Kit. was submitted, after fractionation over silica gel, to a combined analysis by GC(RI), GC/MS and 13C-NMR. The composition was dominated by non terpenic acyclic alcohols and acetates, and phthalides. The main constituents were dodecyl acetate (33.0%), (Z)-ligust...

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Bibliographic Details
Published in:The Journal of essential oil research 2010-05, Vol.22 (3), p.217-219
Main Authors: Bighelli, Ange, Lesueur, Dominique, Casanova, Joseph, Bui Thi Bang, Pham Van Y
Format: Article
Language:English
Subjects:
(Z)-ligustilide
3-(Z)-butylidene-4,5,6,7-tetrahydro-cis-6,7-dihydroxyphtalide
acetates
alcohols
Analytical chemistry
Angelica acutiloba
chemical constituents of plants
Chemical Sciences
dodecanol
dodecyl acetate
essential oil composition
essential oils
gamma-terpinene
gas chromatography
mass spectrometry
medicinal plants
nuclear magnetic resonance spectroscopy
p-cymene
phthalides
quantitative analysis
seeds
terpenoids
tetradecyl acetate
Umbelliferae
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Summary:The seed oil of Angelica acutiloba Kit. was submitted, after fractionation over silica gel, to a combined analysis by GC(RI), GC/MS and 13C-NMR. The composition was dominated by non terpenic acyclic alcohols and acetates, and phthalides. The main constituents were dodecyl acetate (33.0%), (Z)-ligustilide (17.4%), dodecanol (7.1%), p-cymene (6.4%), gamma-terpinene (5.9%) and tetradecyl acetate (5.0%).
ISSN:1041-2905
2163-8152
DOI:10.1080/10412905.2010.9700306