A new high pressure form of Ba3NiSb2O9

In the search of an experimental realization of quantum spin liquid phases we have synthesized polycrystalline samples of Ba3NiSb2O9 under high pressure–high temperature conditions. Combining X-ray powder diffraction, neutron powder diffraction and precession electron diffraction we show that the ob...

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Published in:Journal of solid state chemistry 2016-05, Vol.237, p.166-173
Main Authors: Darie, Céline, Lepoittevin, Christophe, Klein, Holger, Kodjikian, Stéphanie, Bordet, Pierre, Colin, Claire V., Lebedev, Oleg I., Deudon, Catherine, Payen, Christophe
Format: Article
Language:English
Subjects:
Condensed Matter
High pressure–high temperature synthesis
Oxydes
Physics
Quantum spin liquid phases
Strongly Correlated Electrons
TEM
X-ray and neutron diffraction
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cited_by cdi_FETCH-LOGICAL-c378t-f1fbfb006aff285f472e5cdfd7bf74b9189415d9af98f287d7161c549e07ea513
cites cdi_FETCH-LOGICAL-c378t-f1fbfb006aff285f472e5cdfd7bf74b9189415d9af98f287d7161c549e07ea513
container_end_page 173
container_issue
container_start_page 166
container_title Journal of solid state chemistry
container_volume 237
creator Darie, Céline
Lepoittevin, Christophe
Klein, Holger
Kodjikian, Stéphanie
Bordet, Pierre
Colin, Claire V.
Lebedev, Oleg I.
Deudon, Catherine
Payen, Christophe
description In the search of an experimental realization of quantum spin liquid phases we have synthesized polycrystalline samples of Ba3NiSb2O9 under high pressure–high temperature conditions. Combining X-ray powder diffraction, neutron powder diffraction and precession electron diffraction we show that the obtained phase isn't hexagonal as reported in the literature, but trigonal. This new structure shows triangular Ni planes, but only in domains of sizes of the order of 10 nm. It therefore is still interesting as a potential candidate for a quantum spin liquid. Synthesis under high pressure of a new form of Ba3NiSb2O9 : a promising candidate for a quantum spin liquid. Triangular Ni-planes can effectively be present in this structure but only in domains of up to 10nm in size. [Display omitted]
doi_str_mv 10.1016/j.jssc.2016.02.011
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subjects Condensed Matter
High pressure–high temperature synthesis
Oxydes
Physics
Quantum spin liquid phases
Strongly Correlated Electrons
TEM
X-ray and neutron diffraction
title A new high pressure form of Ba3NiSb2O9
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