Multigram Scale Syntheses of First and Second Generation of Trifluoromethanesulfenamide Reagents

Trifluoromethanesulfenamide reagents constitute a family of very efficient reagents to trifluoromethylthiolate various molecules. Optimized syntheses have been developed to easily obtain, in a reproducible manner, large quantities of these reagents, with good overall yields. Up to 84 g have already...

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Bibliographic Details
Published in:Organic process research & development 2016-05, Vol.20 (5), p.960-964
Main Authors: Glenadel, Quentin, Alazet, Sébastien, Baert, François, Billard, Thierry
Format: Article
Language:English
Subjects:
Biochemistry
Biochemistry, Molecular Biology
Chemical Sciences
Life Sciences
Organic chemistry
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Summary:Trifluoromethanesulfenamide reagents constitute a family of very efficient reagents to trifluoromethylthiolate various molecules. Optimized syntheses have been developed to easily obtain, in a reproducible manner, large quantities of these reagents, with good overall yields. Up to 84 g have already been obtained, at a reasonable cost.
ISSN:1083-6160
1520-586X
DOI:10.1021/acs.oprd.6b00062