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Magnetic and Structural Properties of the Nanostructured Cu50Ni50 Powders
Nanocrystalline Cu 50 Ni 50 alloy powder was prepared by the mechanical alloying process in high-energy planetary ball mill P7 under an argon atmosphere. Structural, microstructural, morphological, and magnetic properties were followed by X-ray diffraction, scanning electron microscopy coupled with...
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Published in: | Journal of superconductivity and novel magnetism 2017-07, Vol.30 (7), p.1927-1935 |
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Main Authors: | , , , , |
Format: | Article |
Language: | English |
Subjects: | |
Citations: | Items that this one cites Items that cite this one |
Online Access: | Get full text |
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Summary: | Nanocrystalline Cu
50
Ni
50
alloy powder was prepared by the mechanical alloying process in high-energy planetary ball mill P7 under an argon atmosphere. Structural, microstructural, morphological, and magnetic properties were followed by X-ray diffraction, scanning electron microscopy coupled with EDX analysis, and vibrating sample magnetometry. The mixing of Cu and Ni powders at the atomic level leads to the formation, after 30 h of milling, of two fcc NiCu structures having crystallite sizes of about 15.6 and 65.9 nm and close lattice parameters of about 3.5783 and 3.5794 Ă… that would correspond to Ni
41.8
Cu
58.1
(40.75 %) and Ni
40.6
Cu
59.4
(59.25 %) compositions, respectively. Magnetic measurements reveal that the obtained powders are typical soft magnetic materials. According to the Mr/Ms ratio, the grains are either pseudo-single domain or multidomain. |
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ISSN: | 1557-1939 1557-1947 |
DOI: | 10.1007/s10948-017-4001-0 |