High-Resolution Solid-State Nmr: a Versatile Tool for the Study of AI-O-P Clusters

New Al-O-P clusters are presented. They are characterized by single-crystal X-ray diffraction (XRD) and solid-state NMR. High-resolution techniques such as magic angle spinning (MAS) and multiple quantum magic angle spinning (MQ-MAS) are used. The latest developments of high-resolution 1 H solid-sta...

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Bibliographic Details
Published in:Phosphorus, sulfur, and silicon and the related elements sulfur, and silicon and the related elements, 2001-01, Vol.168 (1), p.243-248
Main Authors: Bonhomme, C., Azaïs, T., Bonhomme-Coury, L., Livage, J., D'Espinose, J-B., Bertani, P., Hirschinger, J., Alonso, B.
Format: Article
Language:English
Subjects:
Al-O-P clusters
Analytical chemistry
Chemical Sciences
high-resolution
Material chemistry
multiple quantum NMR
pictorial representation
solid-state NMR
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Summary:New Al-O-P clusters are presented. They are characterized by single-crystal X-ray diffraction (XRD) and solid-state NMR. High-resolution techniques such as magic angle spinning (MAS) and multiple quantum magic angle spinning (MQ-MAS) are used. The latest developments of high-resolution 1 H solid-state NMR, including very high field and very high speed MAS as well as homonuclear off-resonance Lee-Goldburg (LG) decoupling, are presented. All the experiments are described in the frame of a new pictorial representation of interactions involving quadrics and 4 th degree cartesian surfaces.
ISSN:1042-6507
1563-5325
DOI:10.1080/10426500108546561