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High-pressure, high temperature synthesis of a mesoporous α-quartz/bismuth nanowire composite
High temperature, high pressure conditions were used to insert liquid bismuth in 4–6 nm diameter amorphous silica nanotubes. A combination of transmission electron microscopy and neutron powder diffraction indicate that the final composite consists in 5–6 nm semi-conducting Bi nanowires confined in...
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| Published in: | Solid state sciences 2020-03, Vol.101, p.106125, Article 106125 |
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| Main Authors: | , , , , , , , , , |
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| cites | cdi_FETCH-LOGICAL-c434t-84cb963f3eed61117a3a74a7d651a76c19f2b02fe1678d5455a1360a49a2c8f83 |
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| container_start_page | 106125 |
| container_title | Solid state sciences |
| container_volume | 101 |
| creator | Zhao, Yixuan Talbi, Gaël Clément, Sébastien Toulemonde, Pierre Hansen, Thomas Cambon, Martine Cambon, Olivier Beaudhuin, Mickaël Viennois, Romain Haines, Julien |
| description | High temperature, high pressure conditions were used to insert liquid bismuth in 4–6 nm diameter amorphous silica nanotubes. A combination of transmission electron microscopy and neutron powder diffraction indicate that the final composite consists in 5–6 nm semi-conducting Bi nanowires confined in insulating mesoporous α-quartz. Such a nanostructured material could be of considerable interest for thermoelectric applications.
[Display omitted]
•Bismuth was inserted into 4–6 nm silica nanotubes under high-pressure, high-temperature conditions.•The host amorphous nanotubes crystallize in the form of α-quartz.•The obtained nanocomposite consists of 5–6 nm Bi nanowires imbedded in mesoporous α-quartz.•The formation of Bi nanowires modifies their physical properties compared to bulk Bi. |
| doi_str_mv | 10.1016/j.solidstatesciences.2020.106125 |
| format | article |
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[Display omitted]
•Bismuth was inserted into 4–6 nm silica nanotubes under high-pressure, high-temperature conditions.•The host amorphous nanotubes crystallize in the form of α-quartz.•The obtained nanocomposite consists of 5–6 nm Bi nanowires imbedded in mesoporous α-quartz.•The formation of Bi nanowires modifies their physical properties compared to bulk Bi.</description><identifier>ISSN: 1293-2558</identifier><identifier>EISSN: 1873-3085</identifier><identifier>DOI: 10.1016/j.solidstatesciences.2020.106125</identifier><language>eng</language><publisher>Elsevier Masson SAS</publisher><subject>Bismuth ; Chemical Sciences ; Guest insertion ; High pressure ; Material chemistry ; Nanocomposites ; Silica nanotubes</subject><ispartof>Solid state sciences, 2020-03, Vol.101, p.106125, Article 106125</ispartof><rights>2020 Elsevier Masson SAS</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c434t-84cb963f3eed61117a3a74a7d651a76c19f2b02fe1678d5455a1360a49a2c8f83</citedby><cites>FETCH-LOGICAL-c434t-84cb963f3eed61117a3a74a7d651a76c19f2b02fe1678d5455a1360a49a2c8f83</cites><orcidid>0000-0003-4542-2699 ; 0000-0002-2568-546X ; 0000-0002-7030-3213 ; 0000-0003-4561-5538 ; 0000-0002-8473-8197</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,314,780,784,885,27923,27924</link.rule.ids><backlink>$$Uhttps://hal.umontpellier.fr/hal-02498343$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Zhao, Yixuan</creatorcontrib><creatorcontrib>Talbi, Gaël</creatorcontrib><creatorcontrib>Clément, Sébastien</creatorcontrib><creatorcontrib>Toulemonde, Pierre</creatorcontrib><creatorcontrib>Hansen, Thomas</creatorcontrib><creatorcontrib>Cambon, Martine</creatorcontrib><creatorcontrib>Cambon, Olivier</creatorcontrib><creatorcontrib>Beaudhuin, Mickaël</creatorcontrib><creatorcontrib>Viennois, Romain</creatorcontrib><creatorcontrib>Haines, Julien</creatorcontrib><title>High-pressure, high temperature synthesis of a mesoporous α-quartz/bismuth nanowire composite</title><title>Solid state sciences</title><description>High temperature, high pressure conditions were used to insert liquid bismuth in 4–6 nm diameter amorphous silica nanotubes. A combination of transmission electron microscopy and neutron powder diffraction indicate that the final composite consists in 5–6 nm semi-conducting Bi nanowires confined in insulating mesoporous α-quartz. Such a nanostructured material could be of considerable interest for thermoelectric applications.
[Display omitted]
•Bismuth was inserted into 4–6 nm silica nanotubes under high-pressure, high-temperature conditions.•The host amorphous nanotubes crystallize in the form of α-quartz.•The obtained nanocomposite consists of 5–6 nm Bi nanowires imbedded in mesoporous α-quartz.•The formation of Bi nanowires modifies their physical properties compared to bulk Bi.</description><subject>Bismuth</subject><subject>Chemical Sciences</subject><subject>Guest insertion</subject><subject>High pressure</subject><subject>Material chemistry</subject><subject>Nanocomposites</subject><subject>Silica nanotubes</subject><issn>1293-2558</issn><issn>1873-3085</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNqNUMtOwzAQjBBIlMI_5AgSaf2Kk9yoKqCgSlzgiuU6G-KqqYPXLSp_xY_wTSRqxYULp92dnRlpJoouKRlRQuV4OUK3siUGHQCNhbUBHDHC-rekLD2KBjTPeMJJnh53Oyt4wtI0P43OEJeEECkzMYheZ_atTloPiBsP13HdnXGApgWvQ4fEuFuHGtBi7KpYxw2ga513G4y_v5L3jfbhc7yw2GxCHa_12n3YTmRc0zq0Ac6jk0qvEC4Ocxi93N0-T2fJ_On-YTqZJ0ZwEZJcmEUhecUBSkkpzTTXmdBZKVOqM2loUbEFYRVQmeVlKtJUUy6JFoVmJq9yPoyu9r61XqnW20b7nXLaqtlkrnqMMFHkXPAt7bg3e67xDtFD9SugRPXdqqX6263qu1X7bjuLx70FdJm2Frw60MouvQmqdPb_Zj8kQZEi</recordid><startdate>202003</startdate><enddate>202003</enddate><creator>Zhao, Yixuan</creator><creator>Talbi, Gaël</creator><creator>Clément, Sébastien</creator><creator>Toulemonde, Pierre</creator><creator>Hansen, Thomas</creator><creator>Cambon, Martine</creator><creator>Cambon, Olivier</creator><creator>Beaudhuin, Mickaël</creator><creator>Viennois, Romain</creator><creator>Haines, Julien</creator><general>Elsevier Masson SAS</general><general>Elsevier</general><scope>AAYXX</scope><scope>CITATION</scope><scope>1XC</scope><scope>VOOES</scope><orcidid>https://orcid.org/0000-0003-4542-2699</orcidid><orcidid>https://orcid.org/0000-0002-2568-546X</orcidid><orcidid>https://orcid.org/0000-0002-7030-3213</orcidid><orcidid>https://orcid.org/0000-0003-4561-5538</orcidid><orcidid>https://orcid.org/0000-0002-8473-8197</orcidid></search><sort><creationdate>202003</creationdate><title>High-pressure, high temperature synthesis of a mesoporous α-quartz/bismuth nanowire composite</title><author>Zhao, Yixuan ; Talbi, Gaël ; Clément, Sébastien ; Toulemonde, Pierre ; Hansen, Thomas ; Cambon, Martine ; Cambon, Olivier ; Beaudhuin, Mickaël ; Viennois, Romain ; Haines, Julien</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c434t-84cb963f3eed61117a3a74a7d651a76c19f2b02fe1678d5455a1360a49a2c8f83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Bismuth</topic><topic>Chemical Sciences</topic><topic>Guest insertion</topic><topic>High pressure</topic><topic>Material chemistry</topic><topic>Nanocomposites</topic><topic>Silica nanotubes</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhao, Yixuan</creatorcontrib><creatorcontrib>Talbi, Gaël</creatorcontrib><creatorcontrib>Clément, Sébastien</creatorcontrib><creatorcontrib>Toulemonde, Pierre</creatorcontrib><creatorcontrib>Hansen, Thomas</creatorcontrib><creatorcontrib>Cambon, Martine</creatorcontrib><creatorcontrib>Cambon, Olivier</creatorcontrib><creatorcontrib>Beaudhuin, Mickaël</creatorcontrib><creatorcontrib>Viennois, Romain</creatorcontrib><creatorcontrib>Haines, Julien</creatorcontrib><collection>CrossRef</collection><collection>Hyper Article en Ligne (HAL)</collection><collection>Hyper Article en Ligne (HAL) (Open Access)</collection><jtitle>Solid state sciences</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhao, Yixuan</au><au>Talbi, Gaël</au><au>Clément, Sébastien</au><au>Toulemonde, Pierre</au><au>Hansen, Thomas</au><au>Cambon, Martine</au><au>Cambon, Olivier</au><au>Beaudhuin, Mickaël</au><au>Viennois, Romain</au><au>Haines, Julien</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>High-pressure, high temperature synthesis of a mesoporous α-quartz/bismuth nanowire composite</atitle><jtitle>Solid state sciences</jtitle><date>2020-03</date><risdate>2020</risdate><volume>101</volume><spage>106125</spage><pages>106125-</pages><artnum>106125</artnum><issn>1293-2558</issn><eissn>1873-3085</eissn><abstract>High temperature, high pressure conditions were used to insert liquid bismuth in 4–6 nm diameter amorphous silica nanotubes. A combination of transmission electron microscopy and neutron powder diffraction indicate that the final composite consists in 5–6 nm semi-conducting Bi nanowires confined in insulating mesoporous α-quartz. Such a nanostructured material could be of considerable interest for thermoelectric applications.
[Display omitted]
•Bismuth was inserted into 4–6 nm silica nanotubes under high-pressure, high-temperature conditions.•The host amorphous nanotubes crystallize in the form of α-quartz.•The obtained nanocomposite consists of 5–6 nm Bi nanowires imbedded in mesoporous α-quartz.•The formation of Bi nanowires modifies their physical properties compared to bulk Bi.</abstract><pub>Elsevier Masson SAS</pub><doi>10.1016/j.solidstatesciences.2020.106125</doi><orcidid>https://orcid.org/0000-0003-4542-2699</orcidid><orcidid>https://orcid.org/0000-0002-2568-546X</orcidid><orcidid>https://orcid.org/0000-0002-7030-3213</orcidid><orcidid>https://orcid.org/0000-0003-4561-5538</orcidid><orcidid>https://orcid.org/0000-0002-8473-8197</orcidid><oa>free_for_read</oa></addata></record> |
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| ispartof | Solid state sciences, 2020-03, Vol.101, p.106125, Article 106125 |
| issn | 1293-2558 1873-3085 |
| language | eng |
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| source | ScienceDirect Freedom Collection 2022-2024 |
| subjects | Bismuth Chemical Sciences Guest insertion High pressure Material chemistry Nanocomposites Silica nanotubes |
| title | High-pressure, high temperature synthesis of a mesoporous α-quartz/bismuth nanowire composite |
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