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Effect of double thermal and electrochemical oxidation on titanium alloys for medical applications
[Display omitted] •The nanotube layer is formed on the gas oxidation layers created on the titanium alloy.•The nanotubular structure is strongly dependent on previous gas oxidation.•The colonies of nanotubes of different lengths are observed.•The duplex layer demonstrates good corrosion resistance a...
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Published in: | Applied surface science 2021-10, Vol.563, p.150340, Article 150340 |
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container_title | Applied surface science |
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creator | Ossowska, Agnieszka Olive, Jean-Marc Zieliński, Andrzej Wojtowicz, Andrzej |
description | [Display omitted]
•The nanotube layer is formed on the gas oxidation layers created on the titanium alloy.•The nanotubular structure is strongly dependent on previous gas oxidation.•The colonies of nanotubes of different lengths are observed.•The duplex layer demonstrates good corrosion resistance and biological properties.
The research focuses on the development and characterization of innovative thin hybrid oxide coatings obtained in subsequent processes of thermal (TO) and electrochemical (EO) oxidation. Four different surface modifications were investigated and the microstructure was determined, the mechanical, chemical and biological properties of the Ti-13Nb-13Zr alloy were assessed using scanning electron microscopy, X-ray dispersion analysis, glow discharge emission spectroscopy, Raman spectroscopy, nanoindentation and corrosion resistance measurements. The composite layers were evaluated for antimicrobial activity, cytotoxicity bioassays and wettability tests were performed. The conducted studies of two-stage oxidation (TO + EO) have shown that it is possible to obtain layers with a different structure - crystalline and nanotubular. The formation of a nanotube layer on the surface of the crystalline layer is dependent on the thickness of the crystalline layer. The produced double titanium oxide coatings show high surface roughness, high corrosion resistance, are hydrophilic, slightly antibacterial, and not cytotoxic, which has a huge impact on the process of connecting the tissue with the implant. |
doi_str_mv | 10.1016/j.apsusc.2021.150340 |
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•The nanotube layer is formed on the gas oxidation layers created on the titanium alloy.•The nanotubular structure is strongly dependent on previous gas oxidation.•The colonies of nanotubes of different lengths are observed.•The duplex layer demonstrates good corrosion resistance and biological properties.
The research focuses on the development and characterization of innovative thin hybrid oxide coatings obtained in subsequent processes of thermal (TO) and electrochemical (EO) oxidation. Four different surface modifications were investigated and the microstructure was determined, the mechanical, chemical and biological properties of the Ti-13Nb-13Zr alloy were assessed using scanning electron microscopy, X-ray dispersion analysis, glow discharge emission spectroscopy, Raman spectroscopy, nanoindentation and corrosion resistance measurements. The composite layers were evaluated for antimicrobial activity, cytotoxicity bioassays and wettability tests were performed. The conducted studies of two-stage oxidation (TO + EO) have shown that it is possible to obtain layers with a different structure - crystalline and nanotubular. The formation of a nanotube layer on the surface of the crystalline layer is dependent on the thickness of the crystalline layer. The produced double titanium oxide coatings show high surface roughness, high corrosion resistance, are hydrophilic, slightly antibacterial, and not cytotoxic, which has a huge impact on the process of connecting the tissue with the implant.</description><identifier>ISSN: 0169-4332</identifier><identifier>EISSN: 1873-5584</identifier><identifier>DOI: 10.1016/j.apsusc.2021.150340</identifier><language>eng</language><publisher>Elsevier B.V</publisher><subject>Antibacterial efficiency ; Coatings ; Cytotoxicity ; Electrochemical oxidation ; Engineering Sciences ; Materials ; Microstructure ; Nanoindentation ; Thermal oxidation ; Titanium alloys</subject><ispartof>Applied surface science, 2021-10, Vol.563, p.150340, Article 150340</ispartof><rights>2021 The Authors</rights><rights>Attribution - NonCommercial - NoDerivatives</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c386t-a19aa340806235ee9376d34bb26f7815f09827da586f06cd0c9b4b671fdbfeeb3</citedby><cites>FETCH-LOGICAL-c386t-a19aa340806235ee9376d34bb26f7815f09827da586f06cd0c9b4b671fdbfeeb3</cites><orcidid>0000-0002-4391-9135</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,314,780,784,885,27924,27925</link.rule.ids><backlink>$$Uhttps://hal.science/hal-03483349$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Ossowska, Agnieszka</creatorcontrib><creatorcontrib>Olive, Jean-Marc</creatorcontrib><creatorcontrib>Zieliński, Andrzej</creatorcontrib><creatorcontrib>Wojtowicz, Andrzej</creatorcontrib><title>Effect of double thermal and electrochemical oxidation on titanium alloys for medical applications</title><title>Applied surface science</title><description>[Display omitted]
•The nanotube layer is formed on the gas oxidation layers created on the titanium alloy.•The nanotubular structure is strongly dependent on previous gas oxidation.•The colonies of nanotubes of different lengths are observed.•The duplex layer demonstrates good corrosion resistance and biological properties.
The research focuses on the development and characterization of innovative thin hybrid oxide coatings obtained in subsequent processes of thermal (TO) and electrochemical (EO) oxidation. Four different surface modifications were investigated and the microstructure was determined, the mechanical, chemical and biological properties of the Ti-13Nb-13Zr alloy were assessed using scanning electron microscopy, X-ray dispersion analysis, glow discharge emission spectroscopy, Raman spectroscopy, nanoindentation and corrosion resistance measurements. The composite layers were evaluated for antimicrobial activity, cytotoxicity bioassays and wettability tests were performed. The conducted studies of two-stage oxidation (TO + EO) have shown that it is possible to obtain layers with a different structure - crystalline and nanotubular. The formation of a nanotube layer on the surface of the crystalline layer is dependent on the thickness of the crystalline layer. The produced double titanium oxide coatings show high surface roughness, high corrosion resistance, are hydrophilic, slightly antibacterial, and not cytotoxic, which has a huge impact on the process of connecting the tissue with the implant.</description><subject>Antibacterial efficiency</subject><subject>Coatings</subject><subject>Cytotoxicity</subject><subject>Electrochemical oxidation</subject><subject>Engineering Sciences</subject><subject>Materials</subject><subject>Microstructure</subject><subject>Nanoindentation</subject><subject>Thermal oxidation</subject><subject>Titanium alloys</subject><issn>0169-4332</issn><issn>1873-5584</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp9kF1LwzAUhoMoOKf_wIvcetGZNG2a3ghjzA8YeKPXIZ8sI21K0g33702teCkEEs553kPOA8A9RiuMMH08rMSQjkmtSlTiFa4RqdAFWGDWkKKuWXUJFhlri4qQ8hrcpHRACJe5uwBya61RIwwW6nCU3sBxb2InPBS9hsbnXgxqbzqnci18OS1GF3qYz-hG0btjB4X34ZygDRF2Rv-AYhh8fkxougVXVvhk7n7vJfh83n5sXovd-8vbZr0rFGF0LARuhcgfZ4iWpDamJQ3VpJKypLZhuLaoZWWjRc2oRVRppFpZSdpgq6U1RpIleJjn7oXnQ3SdiGcehOOv6x2falkLI6RqTziz1cyqGFKKxv4FMOKTU37gs1M-OeWz0xx7mmMm73FyJvKknOlV3jpmU1wH9_-AbxV4guQ</recordid><startdate>20211015</startdate><enddate>20211015</enddate><creator>Ossowska, Agnieszka</creator><creator>Olive, Jean-Marc</creator><creator>Zieliński, Andrzej</creator><creator>Wojtowicz, Andrzej</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>6I.</scope><scope>AAFTH</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>1XC</scope><scope>VOOES</scope><orcidid>https://orcid.org/0000-0002-4391-9135</orcidid></search><sort><creationdate>20211015</creationdate><title>Effect of double thermal and electrochemical oxidation on titanium alloys for medical applications</title><author>Ossowska, Agnieszka ; Olive, Jean-Marc ; Zieliński, Andrzej ; Wojtowicz, Andrzej</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c386t-a19aa340806235ee9376d34bb26f7815f09827da586f06cd0c9b4b671fdbfeeb3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Antibacterial efficiency</topic><topic>Coatings</topic><topic>Cytotoxicity</topic><topic>Electrochemical oxidation</topic><topic>Engineering Sciences</topic><topic>Materials</topic><topic>Microstructure</topic><topic>Nanoindentation</topic><topic>Thermal oxidation</topic><topic>Titanium alloys</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ossowska, Agnieszka</creatorcontrib><creatorcontrib>Olive, Jean-Marc</creatorcontrib><creatorcontrib>Zieliński, Andrzej</creatorcontrib><creatorcontrib>Wojtowicz, Andrzej</creatorcontrib><collection>ScienceDirect Open Access Titles</collection><collection>Elsevier:ScienceDirect:Open Access</collection><collection>CrossRef</collection><collection>Hyper Article en Ligne (HAL)</collection><collection>Hyper Article en Ligne (HAL) (Open Access)</collection><jtitle>Applied surface science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ossowska, Agnieszka</au><au>Olive, Jean-Marc</au><au>Zieliński, Andrzej</au><au>Wojtowicz, Andrzej</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effect of double thermal and electrochemical oxidation on titanium alloys for medical applications</atitle><jtitle>Applied surface science</jtitle><date>2021-10-15</date><risdate>2021</risdate><volume>563</volume><spage>150340</spage><pages>150340-</pages><artnum>150340</artnum><issn>0169-4332</issn><eissn>1873-5584</eissn><abstract>[Display omitted]
•The nanotube layer is formed on the gas oxidation layers created on the titanium alloy.•The nanotubular structure is strongly dependent on previous gas oxidation.•The colonies of nanotubes of different lengths are observed.•The duplex layer demonstrates good corrosion resistance and biological properties.
The research focuses on the development and characterization of innovative thin hybrid oxide coatings obtained in subsequent processes of thermal (TO) and electrochemical (EO) oxidation. Four different surface modifications were investigated and the microstructure was determined, the mechanical, chemical and biological properties of the Ti-13Nb-13Zr alloy were assessed using scanning electron microscopy, X-ray dispersion analysis, glow discharge emission spectroscopy, Raman spectroscopy, nanoindentation and corrosion resistance measurements. The composite layers were evaluated for antimicrobial activity, cytotoxicity bioassays and wettability tests were performed. The conducted studies of two-stage oxidation (TO + EO) have shown that it is possible to obtain layers with a different structure - crystalline and nanotubular. The formation of a nanotube layer on the surface of the crystalline layer is dependent on the thickness of the crystalline layer. The produced double titanium oxide coatings show high surface roughness, high corrosion resistance, are hydrophilic, slightly antibacterial, and not cytotoxic, which has a huge impact on the process of connecting the tissue with the implant.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.apsusc.2021.150340</doi><orcidid>https://orcid.org/0000-0002-4391-9135</orcidid><oa>free_for_read</oa></addata></record> |
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subjects | Antibacterial efficiency Coatings Cytotoxicity Electrochemical oxidation Engineering Sciences Materials Microstructure Nanoindentation Thermal oxidation Titanium alloys |
title | Effect of double thermal and electrochemical oxidation on titanium alloys for medical applications |
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