ViscY nuclear magnetic resonance experiments for in situ chemical reaction monitoring under spin diffusion conditions

osity-enhanced spectroscop ( ) offers a new way to analyze complex mixtures of time-varying composition. This communication reports the use of the viscous binary solvent DMSO- /water to induce NMR spin diffusion for chemical reaction monitoring and real-time characterization of a 3-substituted 4-hyd...

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Bibliographic Details
Published in:Analyst (London) 2023-07, Vol.148 (14), p.3179-3183
Main Authors: Pedinielli, François, Leroy, Ritchy, Akrial, Salah-Eddine, Robert, Anthony, Nuzillard, Jean-Marc, Lameiras, Pedro
Format: Article
Language:English
Subjects:
Chemical reactions
Chemical Sciences
Monitoring
NMR
Nuclear magnetic resonance
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Summary:osity-enhanced spectroscop ( ) offers a new way to analyze complex mixtures of time-varying composition. This communication reports the use of the viscous binary solvent DMSO- /water to induce NMR spin diffusion for chemical reaction monitoring and real-time characterization of a 3-substituted 4-hydroxycoumarin derivative and its side-product.
ISSN:0003-2654
1364-5528
DOI:10.1039/d3an00449j