Elastic strain mapping of plastically deformed materials by TEM

• Published in: Ultramicroscopy 2024-11, Vol.265, p.114010, Article 114010
• Main Authors: Després, Arthur, Parent, Salomé, Véron, Muriel, Rauch, Edgar F., Joulain, Anne, Bahsoun, Hadi, Tromas, Christophe
• Format: Article
• Language: English
• Subjects: Condensed Matter; Dislocations; Materials Science; MAX phases; Physics; Strains; Transmission electron microscopy
• ISSN: 0304-3991; 1879-2723; 1879-2723
• DOI: 10.1016/j.ultramic.2024.114010

•Elastic strains maps are measured by TEM in samples with orientation gradients.•The elastic strain around dislocation pile-ups and dislocation walls is clearly distinguished.•With elastic strain maps, the position of the dislocation sources can be inferred. A method for mapping elastic strains by TEM in plastically deformed materials is presented. A characteristic feature of plastically deformed materials, which cannot be handled by standard strain measurement method, is the presence of orientation gradients. To circumvent this issue, we couple orientation and strain maps obtained from scanning precession electron diffraction datasets. More specifically, orientation gradients are taken into account by 1) identifying the diffraction spot positions in a reference pattern, 2) measuring the disorientation between the diffraction patterns in the map and the reference pattern, 3) rotating the coordinate system following the measured disorientation at each position in the map, 4) calculating strains in the rotated coordinate system. At present, only azimuthal rotations of the crystal are handled. The method is illustrated on a Cr2AlC monocrystal micropilar deformed in near simple flexion during a nanomechanical test. After plastic deformation, the sample contains dislocations arranged in pile-ups and walls. The strain-field around each dislocation is consistent with theory, and a clear difference is observed between the strain fields around pile-ups and walls. It is further remarked that strain maps allow for the orientation of the Burgers vector to be identified. Since the loading undergone by the sample is known, this also allows for the position of the dislocation sources to be estimated. Perspectives for the study of deformed materials are finally discussed.