Characterization of anisotropic gas permeability and thermomechanical properties of highly textured porous alumina

• Published in: Journal of the American Ceramic Society 2022-10, Vol.105 (10), p.6335-6344
• Main Authors: Honda, Sawao, Hashimoto, Shinobu, Nait‐Ali, Benoît, Smith, David S., Daiko, Yusuke, Iwamoto, Yuji
• Format: Article
• Language: English
• Subjects: Alumina; Aluminum oxide; Anisotropy; Bend strength; Chemical Sciences; Grain size; Heat conductivity; Heat transfer; Permeability; Platelets; Porosity; porous materials; Room temperature; Sintering (powder metallurgy); Stress analysis; Thermal conductivity; Thermal shock; thermal shock/thermal shock resistance; Thermal stress; Thermomechanical properties
• ISSN: 0002-7820; 1551-2916
• DOI: 10.1111/jace.18573

Porous alumina with a highly textured microstructure was fabricated by pulse electric current sintering (PECS) using alumina platelets. Highly oriented porous alumina with a porosity of 3%–50% was obtained by a pressure‐controlled method of PECS. The properties of the highly textured porous alumina were measured in two directions. The nitrogen gas permeance and thermal conductivity at room temperature were higher in the direction along the platelet length due to the higher continuity of pores and the connectivity of alumina platelets, respectively. The anisotropy of the thermal conductivity at room temperature was investigated and explained by the effect of grain size of platelets as well as morphology and orientation of pores. The bending strength was higher with the loading direction along the platelet thickness. The thermal shock strength was clearly different in the two directions. The difference in the thermal shock strength was investigated by the measurement of properties and thermal stress analysis.