Synthesis of II-VI semiconductor nanoparticles by mechanochemical processing

The synthesis of II-VI semiconductor nanoparticles by mechanochemical reaction has been reviewed. Solid-state displacement reactions between ZnCl/sub 2/ or CdCl/sub 2/ and alkali or alkaline earth chalcogenides were induced during mechanical milling in a steady-state manner, leading to the formation...

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Main Authors: Tsuzuki, T., Nakashima, P.N.H., McCormick, P.G.
Format: Conference Proceeding
Language:English
Subjects:
Crystalline materials
Crystallization
Earth
Lead compounds
Milling
Nanoparticles
Size control
Solid state circuits
Steady-state
Temperature control
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creator Tsuzuki, T.
Nakashima, P.N.H.
McCormick, P.G.
description The synthesis of II-VI semiconductor nanoparticles by mechanochemical reaction has been reviewed. Solid-state displacement reactions between ZnCl/sub 2/ or CdCl/sub 2/ and alkali or alkaline earth chalcogenides were induced during mechanical milling in a steady-state manner, leading to the formation of II-VI semiconductor nanoparticles in a chloride salt matrix. A simple washing process employed to remove the chloride byproduct resulted in separated particles of less than 10 nm. The resulting particles and crystallite sizes were controlled by changing the milling conditions, starting materials, annealing temperature and the presence of a diluent. With decreasing particle size, the band-gap energy and plasmon peak energy of CdS increased due to the quantum confinement effect.
doi_str_mv 10.1109/COMMAD.1998.791674
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Solid-state displacement reactions between ZnCl/sub 2/ or CdCl/sub 2/ and alkali or alkaline earth chalcogenides were induced during mechanical milling in a steady-state manner, leading to the formation of II-VI semiconductor nanoparticles in a chloride salt matrix. A simple washing process employed to remove the chloride byproduct resulted in separated particles of less than 10 nm. The resulting particles and crystallite sizes were controlled by changing the milling conditions, starting materials, annealing temperature and the presence of a diluent. 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With decreasing particle size, the band-gap energy and plasmon peak energy of CdS increased due to the quantum confinement effect.</description><subject>Crystalline materials</subject><subject>Crystallization</subject><subject>Earth</subject><subject>Lead compounds</subject><subject>Milling</subject><subject>Nanoparticles</subject><subject>Size control</subject><subject>Solid state circuits</subject><subject>Steady-state</subject><subject>Temperature control</subject><isbn>9780780345133</isbn><isbn>0780345134</isbn><fulltext>true</fulltext><rsrctype>conference_proceeding</rsrctype><creationdate>1998</creationdate><recordtype>conference_proceeding</recordtype><sourceid>6IE</sourceid><recordid>eNp9js8KgkAYxBciKMoX8LQvoLmp6R6jPyQkHYqusm2fuaG7sp8dfPuMOjcMDPxmDkOIywKfsYAvNqc8X299xnnqJ5ytkmhEHJ6kweAwilkYToiD-AwGRXHMlnxKjudedxWgQmpKmmXeNaMIjZJG31-yM5ZqoU0rbKdkDUhvPW1AVgOT1WcmatpaIwFR6cecjEtRIzi_nBF3v7tsDp4CgKK1qhG2L77Xwr_lG1g4PoM</recordid><startdate>1998</startdate><enddate>1998</enddate><creator>Tsuzuki, T.</creator><creator>Nakashima, P.N.H.</creator><creator>McCormick, P.G.</creator><general>IEEE</general><scope>6IE</scope><scope>6IL</scope><scope>CBEJK</scope><scope>RIE</scope><scope>RIL</scope></search><sort><creationdate>1998</creationdate><title>Synthesis of II-VI semiconductor nanoparticles by mechanochemical processing</title><author>Tsuzuki, T. ; Nakashima, P.N.H. ; McCormick, P.G.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-ieee_primary_7916743</frbrgroupid><rsrctype>conference_proceedings</rsrctype><prefilter>conference_proceedings</prefilter><language>eng</language><creationdate>1998</creationdate><topic>Crystalline materials</topic><topic>Crystallization</topic><topic>Earth</topic><topic>Lead compounds</topic><topic>Milling</topic><topic>Nanoparticles</topic><topic>Size control</topic><topic>Solid state circuits</topic><topic>Steady-state</topic><topic>Temperature control</topic><toplevel>online_resources</toplevel><creatorcontrib>Tsuzuki, T.</creatorcontrib><creatorcontrib>Nakashima, P.N.H.</creatorcontrib><creatorcontrib>McCormick, P.G.</creatorcontrib><collection>IEEE Electronic Library (IEL) Conference Proceedings</collection><collection>IEEE Proceedings Order Plan All Online (POP All Online) 1998-present by volume</collection><collection>IEEE Xplore All Conference Proceedings</collection><collection>IEEE Xplore (Online service)</collection><collection>IEEE Proceedings Order Plans (POP All) 1998-Present</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>Tsuzuki, T.</au><au>Nakashima, P.N.H.</au><au>McCormick, P.G.</au><format>book</format><genre>proceeding</genre><ristype>CONF</ristype><atitle>Synthesis of II-VI semiconductor nanoparticles by mechanochemical processing</atitle><btitle>1998 Conference on Optoelectronic and Microelectronic Materials and Devices. Proceedings (Cat. No.98EX140)</btitle><stitle>COMMAD</stitle><date>1998</date><risdate>1998</risdate><spage>403</spage><epage>406</epage><pages>403-406</pages><isbn>9780780345133</isbn><isbn>0780345134</isbn><abstract>The synthesis of II-VI semiconductor nanoparticles by mechanochemical reaction has been reviewed. Solid-state displacement reactions between ZnCl/sub 2/ or CdCl/sub 2/ and alkali or alkaline earth chalcogenides were induced during mechanical milling in a steady-state manner, leading to the formation of II-VI semiconductor nanoparticles in a chloride salt matrix. A simple washing process employed to remove the chloride byproduct resulted in separated particles of less than 10 nm. The resulting particles and crystallite sizes were controlled by changing the milling conditions, starting materials, annealing temperature and the presence of a diluent. With decreasing particle size, the band-gap energy and plasmon peak energy of CdS increased due to the quantum confinement effect.</abstract><pub>IEEE</pub><doi>10.1109/COMMAD.1998.791674</doi></addata></record>
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identifier ISBN: 9780780345133
ispartof 1998 Conference on Optoelectronic and Microelectronic Materials and Devices. Proceedings (Cat. No.98EX140), 1998, p.403-406
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language eng
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source IEEE Electronic Library (IEL) Conference Proceedings
subjects Crystalline materials
Crystallization
Earth
Lead compounds
Milling
Nanoparticles
Size control
Solid state circuits
Steady-state
Temperature control
title Synthesis of II-VI semiconductor nanoparticles by mechanochemical processing
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