One-Pot Synthesis of Acid Chloride from 1,2-Diols

A simple and mild system for 1,2-diol cleavage has been developed using a combination of lead diacetate and tert-butyl hypochlorite at room temperature.

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Bibliographic Details
Published in:Synthetic communications 2007-03, Vol.37 (5), p.865-868
Main Authors: Telvekar, Vikas N., Mali, Jaishree K., Dighe, Mahesh G.
Format: Article
Language:English
Subjects:
1,2-diols
acid chlorides
aldehydes
lead(II) acetate
tert-butyl hypochlorite
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Description
Summary:A simple and mild system for 1,2-diol cleavage has been developed using a combination of lead diacetate and tert-butyl hypochlorite at room temperature.
ISSN:0039-7911
1532-2432
DOI:10.1080/00397910600978267