N,S-Substituted Dienes from Mono(arylthio)substituted- and S-, S,S-Substituted Dienes

Mono(thio)substituted dienes 1a-1b gave compounds 3a-c and 5d-g with piperazine and piperidine derivatives in dichloromethane. Compounds 8 , 9 , and 10 were obtained from the reactions of perchlorobutadiene ( 6 ) with 1,4-butanedithiol ( 7 ) in ethanol in the presence of sodium hydroxide. Compounds...

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Bibliographic Details
Published in:Phosphorus, sulfur, and silicon and the related elements sulfur, and silicon and the related elements, 2002-12, Vol.177 (12), p.2907-2914
Main Authors: İbiş, Cemil, Gökmen, Zeliha, Bozkurt, Nihal Yilmaz
Format: Article
Language:English
Subjects:
Disulphid
Dithiol
Hexachlorobutadiene
Mono(thio)substituted Nitrodiene
Mono- And Disubstituted Halodienes
N,S-thiosubstituted Nitrodiene
Piperazine
Piperidine
Thioether
Thiol
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Summary:Mono(thio)substituted dienes 1a-1b gave compounds 3a-c and 5d-g with piperazine and piperidine derivatives in dichloromethane. Compounds 8 , 9 , and 10 were obtained from the reactions of perchlorobutadiene ( 6 ) with 1,4-butanedithiol ( 7 ) in ethanol in the presence of sodium hydroxide. Compounds 12a-b , 13a-b were obtained from the reactions of perchlorobutadiene ( 6 ) with allylmercaptan (CH 2 =CH--CH 2 --SH) and mercaptoethanol (HO--CH 2 --CH 2 --SH).
ISSN:1042-6507
1563-5325
DOI:10.1080/10426500214874