N,S-Substituted Nitrodienes from Naphthylthiosubstituted Nitrodienes and S-, S,S-Substituted Dienes from Hexachloro-1,3-Butadiene

Mono(thio)substituted dienes 1 gave compounds 3a-c, 7, 9, and 11 on reaction with pipe-razine derivatives in dry ether. N,S-substtuted nitrodiene 5 was obtained from the reaction of 1 with 1,4-dioxospriol 4. Hexachlorobutadiene 12 in a water-ethanol mixture in the presence of sodium hydroxide reacte...

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Bibliographic Details
Published in:Phosphorus, sulfur, and silicon and the related elements sulfur, and silicon and the related elements, 2007-05, Vol.182 (5), p.1053-1059
Main Authors: İbiş, Cemil, Gökmen, Zeliha
Format: Article
Language:English
Subjects:
hexachloro-1,3-butadiene
N,S-thiosubstituted nitrodiene
Thioether
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Summary:Mono(thio)substituted dienes 1 gave compounds 3a-c, 7, 9, and 11 on reaction with pipe-razine derivatives in dry ether. N,S-substtuted nitrodiene 5 was obtained from the reaction of 1 with 1,4-dioxospriol 4. Hexachlorobutadiene 12 in a water-ethanol mixture in the presence of sodium hydroxide reacted with ethyleneglycol bismercaptoacetate 13 to give thiosubstituted thioethers 14 and 15.
ISSN:1042-6507
1563-5325
DOI:10.1080/10426500601093838